2,5-Bis(benzyloxy)-4-methylbenzaldehyde

Base Information Edit

Chemical Name:2,5-Bis(benzyloxy)-4-methylbenzaldehyde
CAS No.:40930-93-6
Molecular Formula:C22H20O3
Molecular Weight:332.399
Hs Code.:
DSSTox Substance ID:DTXSID10524222
Wikidata:Q82390922
Mol file:40930-93-6.mol

Synonyms:2,5-Bis(benzyloxy)-4-methylbenzaldehyde;40930-93-6;DTXSID10524222

Suppliers and Price of 2,5-Bis(benzyloxy)-4-methylbenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-Bis(benzyloxy)-4-methylbenzaldehyde Edit

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:332.14124450
Heavy Atom Count:25
Complexity:385

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1OCC2=CC=CC=C2)C=O)OCC3=CC=CC=C3

Technology Process of 2,5-Bis(benzyloxy)-4-methylbenzaldehyde

There total 5 articles about 2,5-Bis(benzyloxy)-4-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 91126-02-2
1,4-bis-benzyloxy-2-methylbenzene

: 93-61-8
N-methyl-N-phenylformamide

: 40930-93-6
2,5-bis(benzyloxy)-4-methyl-benzaldehyde

Guidance literature:: With trichlorophosphate; at 60 - 80 ℃; for 3h;
DOI:10.1002/ardp.19843170503

Reference yield:

: 40930-92-5
(2,5-Dibenzyloxy-4-methyl-phenyl)-methanol

: 40930-93-6
2,5-bis(benzyloxy)-4-methyl-benzaldehyde

Guidance literature:: With pyridine; chromium(VI) oxide; In dichloromethane; for 4h;

Reference yield:

: 3899-19-2
2,5-dihydroxy-4-methylbenzoic acid methyl ester

: 40930-93-6
2,5-bis(benzyloxy)-4-methyl-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide

2: LiAlH₄ / diethyl ether / 3 h / Heating

3: CrO₃, Py / CH₂Cl₂ / 4 h

With pyridine; chromium(VI) oxide; lithium aluminium tetrahydride; potassium carbonate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;