Technology Process of Disiloxane, dioxo-
There total 3 articles about Disiloxane, dioxo- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
water;
byproducts: NH3;
- Guidance literature:
-
In
water;
passing of SiHCl3 vapor by a warm O2 stream into H2O of 0 °C;; washing with ice water, alcohol and ether (one after another), drying in a vacuum over P2O5, at least heating and further drying in a desiccator at 110 °C;;
- Guidance literature:
-
With
water; phosphorus pentoxide;
water;
In
neat (no solvent);
byproducts: H2; decompn. reaction with a distinct amount of H2O in P2O5, formation of SiH4 by reaction of nascent H2 with disiloxane, formation of dioxodisiloxane and silicic acid by further hydrolysis;;
