N-(3-Triethoxysilylpropyl)ethylenediamine

Base Information

• Chemical Name: N-(3-Triethoxysilylpropyl)ethylenediamine
• CAS No.: 5089-72-5
• Deprecated CAS: 101964-08-3,159778-18-4,66170-43-2,159778-18-4,66170-43-2
• Molecular Formula: C11H28N2O3Si
• Molecular Weight: 264.44
• Hs Code.: 29319090
• European Community (EC) Number: 225-806-1
• UNII: HZ4EXB3ESF
• DSSTox Substance ID: DTXSID4074647
• Nikkaji Number: J203.293G
• Wikidata: Q72510579
• Mol file: 5089-72-5.mol

Synonyms:5089-72-5;N-(3-Triethoxysilylpropyl)ethylenediamine;N1-(3-(Triethoxysilyl)propyl)ethane-1,2-diamine;N-(2-Aminoethyl)-3-aminopropyltriethoxysilane;3-(2-Aminoethylamino)propyltriethoxysilane;C11H28N2O3Si;N'-(3-triethoxysilylpropyl)ethane-1,2-diamine;1,2-Ethanediamine, N-[3-(triethoxysilyl)propyl]-;N-(3-(Triethoxysilyl)propyl)ethylenediamine;EINECS 225-806-1;1,2-Ethanediamine, N1-[3-(triethoxysilyl)propyl]-;1,2-Ethanediamine, N1-(3-(triethoxysilyl)propyl)-;n-[3-(triethoxysilyl)propyl]ethylenediamine;HZ4EXB3ESF;SCHEMBL18766;DTXSID4074647;C11-H28-N2-O3-Si;aminoethyl aminopropyl triethoxysilane;KH-791;MFCD00138097;AKOS008901326;3-(2-Aminoethylamino)Propyl Triethoxysilane;CS-0205390;FT-0629098;(2-aminoethyl)[3-(triethoxysilyl)propyl]amine;D88485;N-2-(Aminoethyl)-3-AminoPropyltriethoxysilane;S00610;Ethylenediamine, N-[3-(triethoxysilyl)propyl]-;N-(3-(triethoxysilyl)propyl)ethane-1,2-diamine;N1-[3-(Triethoxysilyl)propyl]-1,2-ethanediamine;Silane coupler KH-791;(N-(2-Aminoethyl)-3-aminopropyl)tris-(2-ethoxy)silane;191718-72-6

Chemical Property of N-(3-Triethoxysilylpropyl)ethylenediamine

Chemical Property:

• Appearance/Colour: Colorless clear liquid
• Vapor Pressure: 0.000668mmHg at 25°C
• Melting Point: 135 °C at 5 mmHg
• Refractive Index: 1.438
• Boiling Point: 308.742 °C at 760 mmHg
• PKA: 10.00±0.19(Predicted)
• Flash Point: 140.522 °C
• PSA: 65.74000
• Density: 0.953 g/cm³
• LogP: 2.06440
• Water Solubility.: 240g/L at 20℃
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 12
• Exact Mass: 264.18691929
• Heavy Atom Count: 17
• Complexity: 156

Purity/Quality:

99% ^*data from raw suppliers

N-(2-Aminoethyl)-3-aminopropyltriethoxysilane ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39-24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCO[Si](CCCNCCN)(OCC)OCC

Technology Process of N-(3-Triethoxysilylpropyl)ethylenediamine

There total 2 articles about N-(3-Triethoxysilylpropyl)ethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

→ 3-[N-(2-aminoethyl)]aminopropyltriethoxysilane (5089-72-5)

Guidance literature:

Reference yield:

(3-chloropropyl)triethoxysilane (5089-70-3) + ethylenediamine (107-15-3,85404-18-8) → 3-[N-(2-aminoethyl)]aminopropyltriethoxysilane (5089-72-5)

Guidance literature:

DOI:10.1021/jo00820a011

Reference yield: 96.0%

3-[N-(2-aminoethyl)]aminopropyltriethoxysilane (5089-72-5) + N-Benzyloxycarbonyl-L-proline (1148-11-4) → N,N'-bis[(S)-N-benzyloxycarbonylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine (502186-02-9)

Guidance literature:

N-Benzyloxycarbonyl-L-proline; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 5 - 10 ℃; for 0.5h;

3-[N-(2-aminoethyl)]aminopropyltriethoxysilane; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1016/S0022-328X(02)01469-9

upstream raw materials:

(3-chloropropyl)triethoxysilane

ethylenediamine

Downstream raw materials:

N,N'-bis[(S)-N-benzylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

N,N'-bis[(S)-N-benzyloxycarbonylprolyl]-N-(2-aminoethyl-3-aminopropyl)triethoxysilylethylenediamine

2-cyanoethyltriethoxysilane

Refernces

• 1、 -. "Fluorescent probe and fluorescence detecting method". . . Retrieved 2008/06/13.
• 2、 -. "Method and apparatus for preparing 3-[N-(2-aminoethyl)]aminopropylalkoxysilane". . . Retrieved 2008/06/13.