Technology Process of O-Mannopyranosylserine
There total 4 articles about O-Mannopyranosylserine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2 / 10percent Pd-C / methanol / 5 h / 3000.2 Torr
2: hydrazine hydrate / methanol / 2 h / Ambient temperature
With
hydrogen; hydrazine hydrate;
palladium on activated charcoal;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 60 percent / morpholine / 0.5 h / Ambient temperature
2: H2 / 10percent Pd-C / methanol / 5 h / 3000.2 Torr
3: hydrazine hydrate / methanol / 2 h / Ambient temperature
With
morpholine; hydrogen; hydrazine hydrate;
palladium on activated charcoal;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 89 percent / silver triflate, 4A molecular sieves / toluene; CH2Cl2 / 1) 0 deg C to room temperature, 2) room temperature, 1 h
2: 60 percent / morpholine / 0.5 h / Ambient temperature
3: H2 / 10percent Pd-C / methanol / 5 h / 3000.2 Torr
4: hydrazine hydrate / methanol / 2 h / Ambient temperature
With
morpholine; 4 A molecular sieve; hydrogen; silver trifluoromethanesulfonate; hydrazine hydrate;
palladium on activated charcoal;
In
methanol; dichloromethane; toluene;
