Technology Process of Phenol, 2-[[8-[bis(2-hydroxyethyl)amino]octyl]oxy]-
There total 4 articles about Phenol, 2-[[8-[bis(2-hydroxyethyl)amino]octyl]oxy]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
ethanol; ethyl acetate;
for 20h;
under 1794.37 - 3759.59 Torr;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / tetrahydrofuran / 92 h / 25 °C / Heating / reflux
2: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 20 h / 1794.37 - 3759.59 Torr
With
hydrogen; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / ethanol / 25.5 h / 25 °C / Heating / reflux
2: triethylamine / tetrahydrofuran / 92 h / 25 °C / Heating / reflux
3: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 20 h / 1794.37 - 3759.59 Torr
With
hydrogen; potassium carbonate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; ethyl acetate;
