3-METHOXY-2-BUTANOL

Base Information

• Chemical Name: 3-METHOXY-2-BUTANOL
• CAS No.: 53778-72-6
• Molecular Formula: C5H12O2
• Molecular Weight: 104.149
• Hs Code.: 2909499000
• Mol file: 53778-72-6.mol

Synonyms:2-Butanol, 3-methoxy-;2.3-Butylenglykol-monomethylaether;2.3-butylene glycol-monomethyl ether;3-Methoxy-2-butanol;2-Butanol,3-methoxy;2-methoxy-3-butanol;

Chemical Property of 3-METHOXY-2-BUTANOL

Chemical Property:

• Boiling Point: 134-136 °C
• PKA: 14.51±0.20(Predicted)
• PSA: 29.46000
• Density: 0.9186 g/cm3(Temp: 15 °C)
• LogP: 0.40210
• Storage Temp.: 2-8°C

Purity/Quality:

98%Min ^*data from raw suppliers

3-Methoxy-2-butanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-METHOXY-2-BUTANOL

There total 14 articles about 3-METHOXY-2-BUTANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 2,3-cis-epoxybutane (925669-95-0) → 2-Methoxybutanol-(3) (threo) (53778-72-6,54389-81-0,54389-82-1,80185-56-4)

Guidance literature:

With sulfuric acid;

Reference yield:

methanol (67-56-1) + 2,3-cis-epoxybutane (925669-95-0) → 2-methoxy-3-butanol (53778-72-6)

Guidance literature:

With Titanium substituted ZSM-5; dihydrogen peroxide; at 30 ℃; for 4h;

DOI:10.1006/jcat.1994.1285

Reference yield:

methanol (67-56-1) + 2,3-trans-epoxybutane (21490-63-1) → 2-Methoxybutanol-(3) (erythro) (53778-72-6,54389-81-0,54389-82-1,80185-56-4)

Guidance literature:

With sulfuric acid;

upstream raw materials:

methanol

2,3-cis-epoxybutane

2,3-trans-epoxybutane

2-chloro-3-methoxy-butane

Downstream raw materials:

buta-1,3-diene

Refernces

• 1、 Sung, Jin Hong,Jin, Soo Seo,Ji, Young Ryu,Jung, Hwan Lee,Kim, Cheal,Kim, Sung-Jin,Kim, Youngmee,Lough, Alan J.. "Structure and heterogeneous catalytic activity of a coordination polymer containing Cu(NO3)2 and Cu(H2O) 22+ units bridged alternatively by btp ligands (btp=2,6-bis(N′-1,2,4-triazolyl)pyridine)". . p. 22 - 28. Retrieved 2007/10/03.
• 2、 Yoo, Dong-Woo,Yoo, Sang-Kun,Kim, Cheal,Lee, Jin-Kyu. "A novel mononuclear Fe(III) mono(terpyridine) complex having labile solvent ligands and its catalytic activity". . p. 3931 - 3932. Retrieved 2007/10/03.