Benzoic acid, 3,4-diamino-5-nitro-

Base Information

• Chemical Name: Benzoic acid, 3,4-diamino-5-nitro-
• CAS No.: 54226-22-1
• Molecular Formula: C7H7N3O4
• Molecular Weight: 197.15
• Mol file: 54226-22-1.mol

Synonyms:

Chemical Property of Benzoic acid, 3,4-diamino-5-nitro-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 3,4-diamino-5-nitro-

There total 6 articles about Benzoic acid, 3,4-diamino-5-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-amino-3,5-dinitrobenzoic acid (7221-27-4) → 3,4-diamino-5-nitrobenzoic acid (54226-22-1)

Guidance literature:

4-amino-3,5-dinitrobenzoic acid; With nitrogen; palladium 10% on activated carbon; In Dimethyl ether; chloroform; for 15h; under 1810.07 Torr;

With hydrogen; palladium 10% on activated carbon; In Dimethyl ether; chloroform; for 15h; under 1810.07 Torr;

Reference yield:

4-chloro-3,5-dinitrobenzoic acid (118-97-8) → 3,4-diamino-5-nitrobenzoic acid (54226-22-1)

Guidance literature:

With ammonia; Einleiten von Schwefelwasserstoff in die erhaltene Suspension;

Reference yield:

para-chlorobenzoic acid (74-11-3) → 3,4-diamino-5-nitrobenzoic acid (54226-22-1)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid; potassium nitrate / 2 h / 125 °C / High pressure

2: ammonium hydroxide / methanol / 19.5 h / 20 °C / Reflux

3: sodium sulfide; sodium hydrogencarbonate / water / 1 h / 60 - 75 °C

With sodium sulfide; ammonium hydroxide; sulfuric acid; sodium hydrogencarbonate; potassium nitrate; In methanol; water;

DOI:10.3390/molecules25204751

upstream raw materials:

4-amino-3,5-dinitrobenzoic acid

4-chloro-3,5-dinitrobenzoic acid

para-chlorobenzoic acid

Refernces

• 1、 -. "HYDROXYETHYLAMINE DERIVATIVES FOR THE TREATMENT OF ALZHEIMER'S DISEASE". Page 65. . Retrieved 2010/02/07.