OctanaMide, N-(phenylMethyl)-

Base Information

• Chemical Name: OctanaMide, N-(phenylMethyl)-
• CAS No.: 70659-87-9
• Molecular Formula: C15H23NO
• Molecular Weight: 233.354
• Mol file: 70659-87-9.mol

Synonyms:N-benzylstearamide;N-Benzyl-octansaeureamid;N-Benzyl-stearamid;N-benzyloctanoic amide;N-benzyl-octadecanamide;N-octadecanoyl benzylamine;N-Benzyl-stearinamid;N-Benzyl-octanamid;N-benzyl octanamide;

Chemical Property of OctanaMide, N-(phenylMethyl)-

Chemical Property:

• Vapor Pressure: 1.02E-06mmHg at 25°C
• Boiling Point: 403.3°Cat760mmHg
• Flash Point: 245.5°C
• PSA: 29.10000
• Density: 0.957g/cm³
• LogP: 4.05420

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of OctanaMide, N-(phenylMethyl)-

There total 23 articles about OctanaMide, N-(phenylMethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C16H25NO2 → N-benzyloctanoic amide (70659-87-9)

Guidance literature:

With chloro-trimethyl-silane; sodium iodide; In acetonitrile; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2020.131630

Reference yield: 98.0%

Octanal (124-13-0) + benzylamine (100-46-9) → octyl octylate (2306-88-9) + N-benzyloctanoic amide (70659-87-9) + N‐benzyloctan‐1‐imine (161643-01-2)

Guidance literature:

With potassium phosphate; Rh(trop2NH)(PPh₃)(OTf); methacrylic acid methyl ester; In tetrahydrofuran; at 0 ℃;

DOI:10.1002/cctc.201200495

Reference yield: 98.0%

Octanoic acid (124-07-2) + benzylamine (100-46-9) → N-benzyloctanoic amide (70659-87-9)

Guidance literature:

polystyrene-bound pyridine-3-boronic acid; In toluene; for 20h; Heating;

DOI:10.1055/s-2001-16758

upstream raw materials:

Octanoic acid

benzylamine

octanoic acid ethyl ester

benzyl caprylate

Downstream raw materials:

N‐benzyloctan‐1‐imine

Refernces

• 1、 Achard, Thierry,Bellemin-Laponnaz, Stéphane,Chen, Weighang,Egly, Julien,Maisse-Fran?ois, Aline. "Half-Sandwich Ruthenium Complexes Bearing Hemilabile κ2-(C,S)?Thioether-Functionalized NHC Ligands: Application to Amide Synthesis from Alcohol and Amine". supporting information. . Retrieved 2022/01/20.
• 2、 Wang, Hui,Dong, Wei,Hou, Zhipeng,Cheng, Lidan,Li, Xiufen,Huang, Longjiang. "Direct amidation of non-activated carboxylic acid and amine derivatives catalyzed by TiCp2Cl2". . . Retrieved 2020/02/15.