1-(2-Bromoethyl)piperidine hydrobromide

Base Information

• Chemical Name: 1-(2-Bromoethyl)piperidine hydrobromide
• CAS No.: 89796-22-5
• Molecular Formula: C7H14BrN
• Molecular Weight: 273.011
• Hs Code.: 2933399090
• European Community (EC) Number: 818-642-2
• DSSTox Substance ID: DTXSID60498363
• NSC Number: 194924
• Mol file: 89796-22-5.mol

Synonyms:1-(2-Bromoethyl)piperidine hydrobromide;89796-22-5;1-(2-Bromoethyl)piperidine HBr;1-(2-bromoethyl)piperidine;hydrobromide;MFCD00463352;1-(2-Bromoethyl)piperidineHydrobromide;1-(2-Bromo-ethyl)-piperidine hydrobromide;Piperidine, 1-(2-bromoethyl)-, hydrobromide;SCHEMBL1846886;DTXSID60498363;RIOIXQFVMBDUGI-UHFFFAOYSA-N;NSC194924;AKOS016008831;CS-W005524;DS-4642;NSC-194924;SY040485;FT-0711107;EN300-74506;O10261;1-(2-Bromoethyl)piperidine--hydrogen bromide (1/1)

Chemical Property of 1-(2-Bromoethyl)piperidine hydrobromide

Chemical Property:

• Vapor Pressure: 0.23mmHg at 25°C
• Melting Point: 219-220 °C(Solv: ethanol (64-17-5))
• Boiling Point: 207°Cat760mmHg
• Flash Point: 79°C
• PSA: 3.24000
• Density: 1.295g/cm³
• LogP: 2.76320
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 272.95508
• Heavy Atom Count: 10
• Complexity: 69.3

Purity/Quality:

96% 1H NMR ^*data from raw suppliers

1-(2-Bromoethyl)piperidinehydrobromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCN(CC1)CCBr.Br

Technology Process of 1-(2-Bromoethyl)piperidine hydrobromide

There total 4 articles about 1-(2-Bromoethyl)piperidine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

→ β-Piperidinoethyl bromide hydrobromide (89796-22-5) + 1-Piperidino-2-phenoxyethane (74-41-9)

Guidance literature:

Reference yield: 73.0%

1-piperidinoethanol (3040-44-6) → β-Piperidinoethyl bromide hydrobromide (89796-22-5)

Guidance literature:

With hydrogen bromide;

DOI:10.1039/c6cc04619c

Reference yield:

piperidine (110-89-4) → β-Piperidinoethyl bromide hydrobromide (89796-22-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HBr / toluene

With hydrogen bromide; In toluene;

DOI:10.1071/CH07010

upstream raw materials:

1-piperidinoethanol

piperidine

Downstream raw materials:

N'-((5-cyanopyrazolo[1,5-a]pyridin-3-yl)methylene)-2-methyl-5-nitro-N-(2-(piperidin-1-yl)ethyl)benzenesulfonohydrazide

Refernces

• 1、 Okimoto, Mitsuhiro,Yoshida, Takashi,Hoshi, Masayuki,Hattori, Kazuyuki,Komata, Masashi,Numata, Kaori,Tomozawa, Kenta. "Electrooxidative cyclization of hydroquinolyl alcohols, hydroquinolylamines, and dimethyl aminomalonates". . p. 236 - 242. Retrieved 2008/02/11.
• 2、 -. "Aminoindazole derivatives". . . Retrieved 2008/06/13.