Ethanone, 1-[3-[(2,3-dihydro-5-methyl-7-nitro-1H-inden-4-yl)oxy]-2-hydroxy-6-(phen ylmethoxy)phenyl]-

Base Information

• Chemical Name: Ethanone, 1-[3-[(2,3-dihydro-5-methyl-7-nitro-1H-inden-4-yl)oxy]-2-hydroxy-6-(phen ylmethoxy)phenyl]-
• CAS No.: 575504-75-5
• Molecular Formula: C25H23NO6
• Molecular Weight: 433.461
• Mol file: 575504-75-5.mol

Synonyms:

Chemical Property of Ethanone, 1-[3-[(2,3-dihydro-5-methyl-7-nitro-1H-inden-4-yl)oxy]-2-hydroxy-6-(phen ylmethoxy)phenyl]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ethanone, 1-[3-[(2,3-dihydro-5-methyl-7-nitro-1H-inden-4-yl)oxy]-2-hydroxy-6-(phen ylmethoxy)phenyl]-

There total 1 articles about Ethanone, 1-[3-[(2,3-dihydro-5-methyl-7-nitro-1H-inden-4-yl)oxy]-2-hydroxy-6-(phen ylmethoxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[2,6-Bis-benzyloxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone (575504-42-6) + water (7732-18-5) → 1-[6-Benzyloxy-2-hydroxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone (575504-75-5)

Guidance literature:

1-[2,6-Bis-benzyloxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone; With sodium bicarbonate; trifluoroacetic acid; In dichloromethane; water; dimethyl sulfoxide; at 20 ℃; for 12h;

water;

Reference yield:

1-[6-Benzyloxy-2-hydroxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone (575504-75-5) → 1-[6-Benzyloxy-2-methoxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone (575505-06-5)

Guidance literature:

With caesium carbonate; methyl iodide; In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield:

1-[6-Benzyloxy-2-hydroxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone (575504-75-5) + hexane (110-54-3) → ethyl N'-{1-[6-benzyloxy-2-hydroxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethylidene}hydrazinecarboxate

Guidance literature:

1-[6-Benzyloxy-2-hydroxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone; With ethylhydrazine carboxylate; In propan-1-ol; at 75 ℃; for 12h;

hexane; In propan-1-ol; at 20 ℃; for 1h;

upstream raw materials:

1-[2,6-Bis-benzyloxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone

water

Downstream raw materials:

1-[6-Benzyloxy-2-methoxy-3-(5-methyl-7-nitroindan-4-yloxy)phenyl]ethanone

3-Benzyloxy-2-ethyl-6-(5-methyl-7-nitroindan-4-yloxy)phenol

Refernces