methyl dibutoxyphosphanecarboxylate oxide

Base Information

• Chemical Name: methyl dibutoxyphosphanecarboxylate oxide
• CAS No.: 72304-81-5
• Molecular Formula: C10H21O5P
• Molecular Weight: 252.2445
• Mol file: 72304-81-5.mol

Synonyms:Phosphinecarboxylic acid,dibutoxy-,methyl ester,oxide;methyl dibutoxyphosphinecarboxylate oxide;di-n-butyl (methoxycarbonyl)phosphonate;

Chemical Property of methyl dibutoxyphosphanecarboxylate oxide

Chemical Property:

• Vapor Pressure: 0.00042mmHg at 25°C
• Boiling Point: 316.1°Cat760mmHg
• Flash Point: 158.8°C
• PSA: 71.64000
• Density: 1.078g/cm³
• LogP: 3.57930

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl dibutoxyphosphanecarboxylate oxide

There total 1 articles about methyl dibutoxyphosphanecarboxylate oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

tri-n-butyl phosphite (102-85-2) + methyl chloroformate (79-22-1) → di-n-butyl methoxycarbonylphosphonate (72304-81-5)

Guidance literature:

DOI:10.1021/jm00356a028

Reference yield: 14.0%

di-n-butyl methoxycarbonylphosphonate (72304-81-5) → Sodium n-butyl methoxycarbonylphosphonate (72304-93-9)

Guidance literature:

With sodium iodide; In tetrahydrofuran; for 96h;

DOI:10.1021/jm00356a028

Reference yield:

di-n-butyl methoxycarbonylphosphonate (72304-81-5) → b-butyl sodium phosphite (56317-58-9)

Guidance literature:

With sodium hydroxide; for 1h; Heating;

DOI:10.1021/jm00356a028

upstream raw materials:

tri-n-butyl phosphite

methyl chloroformate

Downstream raw materials:

b-butyl sodium phosphite

Sodium n-butyl methoxycarbonylphosphonate

Refernces

• 1、 -. "Phosphonoformic acid esters and pharmaceutical compositions containing same". . . Retrieved 2008/06/13.