1,1,4,4-tetramethylpiperazinediium dibromide

Base Information

• Chemical Name: 1,1,4,4-tetramethylpiperazinediium dibromide
• CAS No.: 24996-75-6
• Molecular Formula: 2Br*C₈H₂₀N₂
• Molecular Weight: 304.068
• Mol file: 24996-75-6.mol

Synonyms:1,1,4,4-Tetramethylpiperaziniumdibromide (6CI); Piperazinium, 1,1,4,4-tetramethyl-, dibromide (8CI,9CI)

Chemical Property of 1,1,4,4-tetramethylpiperazinediium dibromide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1,4,4-tetramethylpiperazinediium dibromide

There total 5 articles about 1,1,4,4-tetramethylpiperazinediium dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(N,N-dimethylamino)ethyl bromide (5459-68-7) → 1,1,4,4-tetramethylpiperazinium dibromide (24996-75-6)

Guidance literature:

With potassium carbonate; alloxazine; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;

DOI:10.1002/chem.201600207

Reference yield:

N,N,N,N,-tetramethylethylenediamine (110-18-9) + ethylene dibromide (106-93-4) → 1,1,4,4-tetramethylpiperazinium dibromide (24996-75-6)

Guidance literature:

With ethanol;

Reference yield:

1,5-dibromo-pentane (111-24-0) + bis-(dimethylamino)methane (51-80-9) → 1,1,4,4-tetramethylpiperazinium dibromide (24996-75-6)

Guidance literature:

In acetonitrile; Ambient temperature;

DOI:10.1246/bcsj.61.999

upstream raw materials:

N,N'-dimethylpiperazine

methyl bromide

N,N,N,N,-tetramethylethylenediamine

ethylene dibromide

Refernces

• 1、 Kormányos, Attila,Hossain, Mohammad S.,Ghadimkhani, Ghazaleh,Johnson, Joe J.,Janáky, Csaba,de Tacconi, Norma R.,Foss, Frank W.,Paz, Yaron,Rajeshwar, Krishnan. "Flavin Derivatives with Tailored Redox Properties: Synthesis, Characterization, and Electrochemical Behavior". . p. 9209 - 9217. Retrieved 2016.