2,3-Dichloroanthracene

Base Information

• Chemical Name: 2,3-Dichloroanthracene
• CAS No.: 613-07-0
• Molecular Formula: C14H8Cl2
• Molecular Weight: 247.124
• Mol file: 613-07-0.mol

Synonyms:Anthracene, 2,3-dichloro-;

Chemical Property of 2,3-Dichloroanthracene

Chemical Property:

• Melting Point: 261 °C
• Boiling Point: 402.6±18.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.361±0.06 g/cm3(Predicted)
• LogP: 5.29980

Purity/Quality:

98%min ^*data from raw suppliers

2,3-DICHLOROANTHRACENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-Dichloroanthracene

There total 8 articles about 2,3-Dichloroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2,3-dichloro-anthraquinone (84-45-7) → 2,3-dichloroanthracene (613-07-0)

Guidance literature:

With ammonium hydroxide; zinc; In water; for 96h; Reflux;

Reference yield: 80.0%

2,3-dichloro-9,10-dihydroanthracene → 2,3-dichloroanthracene (613-07-0)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 4h; Reflux;

DOI:10.1021/acs.joc.9b01567

Reference yield:

2,3-dichloroanthrone (52075-62-4) → 2,3-dichloroanthracene (613-07-0)

Guidance literature:

With potassium hydroxide; zinc;

upstream raw materials:

2,3-dichloroanthrone

1,2,3,4-tetrachloro-9,10-anthraquinone

2,3-dichloro-anthraquinone

copper(II) sulfate

Downstream raw materials:

1,2-dihydroxy-9,10-anthracenedione

2,3-dichloro-anthraquinone

Refernces

• 1、 Singh, M. Dhaneshwar,Ningombam, Anjana. "Diels-Alder reaction of 9-anthracenemethanol and dimethylacetylene- dicarboxylate; potential route for the synthesis of regiospecific products of 9-substituted anthracene with unsymmetrical acetylenes". experimental part. p. 77 - 83. Retrieved 2010/04/26.