(4-Iodophenyl)hydrazine hydrochloride

Base Information

• Chemical Name: (4-Iodophenyl)hydrazine hydrochloride
• CAS No.: 62830-55-1
• Molecular Formula: C6H7IN2.ClH
• Molecular Weight: 270.5
• Hs Code.: 2928000090
• European Community (EC) Number: 832-872-0
• Mol file: 62830-55-1.mol

Synonyms:(4-iodophenyl)hydrazine hydrochloride;62830-55-1;4-Iodophenylhydrazine hydrochloride;4-Iodophenylhydrazine, HCl;(4-iodophenyl)hydrazine;hydrochloride;(4-Iodophenyl)hydrazine HCl;MFCD00060724;HYDRAZINE, (4-IODOPHENYL)-, MONOHYDROCHLORIDE;SCHEMBL379453;PBGQZFXOUDOZCB-UHFFFAOYSA-N;(4-iodophenyl)hydrazinehydrochloride;AKOS001475845;DS-15606;SY046538;CS-0157466;EN300-1663795;A868350

Chemical Property of (4-Iodophenyl)hydrazine hydrochloride

Chemical Property:

• PSA: 38.05000
• LogP: 3.15210
• Storage Temp.: 2-8°C(protect from light)
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 269.94207
• Heavy Atom Count: 10
• Complexity: 79.1

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-IodophenylhydrazineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1NN)I.Cl

Technology Process of (4-Iodophenyl)hydrazine hydrochloride

There total 1 articles about (4-Iodophenyl)hydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-aminoiodobenzene (540-37-4) → 2-(4-iodophenyl)hydrazin-1-ium chloride (62830-55-1)

Guidance literature:

With hydrogenchloride; tin(II) chloride dihdyrate; sodium nitrite; In water; at -20 - -5 ℃; for 0.75h;

DOI:10.1016/j.ejmech.2011.01.075

Reference yield: 92.0%

4,4,4-trifluoro-1-(4-methylphenyl)butane-1,3-dione (720-94-5) + 2-(4-iodophenyl)hydrazin-1-ium chloride (62830-55-1) → 1-(4-iodophenyl)-5-(p-tolyl)-3-(trifluoromethyl)-1H-pyrazole

Guidance literature:

In acetic acid; at 80 ℃; for 15h; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.201901874

Reference yield: 87.0%

2-(4-iodophenyl)hydrazin-1-ium chloride (62830-55-1) + N-(4-oxo-5-phenylpentyl)acetamide (823821-72-3) → N-[3-(5-iodo-3-phenyl-1H-indol-2-yl)-propyl]-acetamide

Guidance literature:

In ethanol; Heating;

DOI:10.1070/MC2006v016n04ABEH002280

upstream raw materials:

p-aminoiodobenzene

Downstream raw materials:

10-(4-Iodo-phenyl)-10H-7-thia-10,11-diaza-cyclohepta[a]naphthalene-5,9-dione

{1-[(4-Iodo-phenyl)-hydrazono]-3-methyl-4-oxo-1,4-dihydro-naphthalen-2-yloxy}-acetic acid ethyl ester

10-(4-Iodo-phenyl)-6-methyl-10H-7-thia-10,11-diaza-cyclohepta[a]naphthalene-5,9-dione

{1-[(4-Iodo-phenyl)-hydrazono]-3-methyl-4-oxo-1,4-dihydro-naphthalen-2-ylsulfanyl}-acetic acid ethyl ester

Refernces

• 1、 Lee, Se Hoon,Mergu, Naveen,Min, Kyeong Su,Satish Kumar, Rangaraju,Son, Young-A. "Synthesis of novel panchromatic porphyrin-squaraine dye and application towards TiO2 combined photocatalysis". . . Retrieved 2020/05/13.
• 2、 -. "ASYMMETRIC TRIAZOLE BENZAMIDE DERIVATIVES AND THE COMPOSITIONS AND METHODS OF TREATMENT REGARDING THE SAME". Paragraph 676; 677. . Retrieved 2019/06/17.