Di(p-toluidinomethyl)phenylphosphine oxide

Base Information

• Chemical Name: Di(p-toluidinomethyl)phenylphosphine oxide
• CAS No.: 85684-51-1
• Molecular Formula: C₂₂H₂₅N₂OP
• Molecular Weight: 364.427
• Mol file: 85684-51-1.mol

Synonyms:

Chemical Property of Di(p-toluidinomethyl)phenylphosphine oxide

Chemical Property:

• Boiling Point: 618.8°Cat760mmHg
• Flash Point: 328°C
• Density: 1.15g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Di(p-toluidinomethyl)phenylphosphine oxide

There total 1 articles about Di(p-toluidinomethyl)phenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

p-toluidine (106-49-0,12221-03-3) + bis(hydroxymethyl)phenylphosphine (3127-08-0) → di(p-tolylaminomethyl)phenylphosphine oxide (85684-51-1)

Guidance literature:

With dihydrogen peroxide; In acetone; for 2h;

DOI:10.1007/BF00765168

Reference yield: 55.0%

di(p-tolylaminomethyl)phenylphosphine oxide (85684-51-1) + methyl iodide (74-88-4) → C23H27N2OP*HI

Guidance literature:

at 40 ℃; for 2h;

DOI:10.1007/BF00953167

upstream raw materials:

p-toluidine

bis(hydroxymethyl)phenylphosphine

Refernces

• 1、 Molodykh, Zh. V.,Anisimova, N. N.,Kudrina, M. A.,Loseva, M. S.,Nikonov, G. N.,Erastov, O. A.. "ANTIMICROBIAL ACTIVITY OF CERTAIN DERIVATIVES OF PHOSPHINE AND PHENYLPHOSPHINE". . p. 206 - 210. Retrieved 2007/10/02.