benzeneindone

Base Information

• Chemical Name: benzeneindone
• CAS No.: 641-30-5
• Molecular Formula: C18H12N2O
• Molecular Weight: 272.306
• Hs Code.: 2933990090
• Mol file: 641-30-5.mol

Synonyms:2(10H)-Phenazinone, 10-phenyl-;10-phenyl-10H-phenazin-2-one;3-hydroxy-5-phenyl-phenazinium betaine;3-Hydroxy-5-phenyl-phenazinium-betain;10-Phenylphenazin-2-on;aposafranone;Aposafranon;

Chemical Property of benzeneindone

Chemical Property:

• PSA: 34.89000
• LogP: 3.53890

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzeneindone

There total 15 articles about benzeneindone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

3-phenylaminocyclohex-2-enone (24706-50-1) + ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → aposafranone (641-30-5)

Guidance literature:

With caesium carbonate; In dimethyl sulfoxide; at 20 ℃;

DOI:10.1021/acs.orglett.1c00710

Reference yield:

3-dimethylamino-5-phenyl-phenazinium; hydroxide → aposafranone (641-30-5) + dimethyl amine (124-40-3)

Guidance literature:

Reference yield:

→ aposafranone (641-30-5)

Guidance literature:

With water; at 180 ℃; unter Druck;

upstream raw materials:

5-phenyl-5,10-dihydro-phenazine

hydroxyquinone

acetic acid

N-phenyl-1,2-benzenediamine

Downstream raw materials:

8,10-dihydro-1-iodo-10-phenylphenazin-2(7H)-one

3-hydroxy-5-phenyl-2-(2,4,6,N-tetrabromo-anilino)-phenazinium betaine

3-hydroxy-5-phenyl-2-(2,4,6-tribromo-anilino)-phenazinium-betaine

2-phenylamino-5-phenyl-3-phenazinone

Refernces