(6-Bromohexyl)diethylamine hydrobromide

Base Information

• Chemical Name: (6-Bromohexyl)diethylamine hydrobromide
• CAS No.: 64993-14-2
• Molecular Formula: C10H22BrN.BrH
• Molecular Weight: 317.107
• European Community (EC) Number: 629-911-7
• DSSTox Substance ID: DTXSID70892439
• Mol file: 64993-14-2.mol

Synonyms:64993-14-2;(6-bromohexyl)diethylamine hydrobromide;SCHEMBL2929563;DTXSID70892439;E80309;6-Bromo-N,N-diethyl-1-hexanamine hydrobromide (1:1)

Chemical Property of (6-Bromohexyl)diethylamine hydrobromide

Chemical Property:

• PSA: 3.24000
• LogP: 4.08550
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 8
• Exact Mass: 317.01768
• Heavy Atom Count: 13
• Complexity: 81.9

Purity/Quality:

99%min ^*data from raw suppliers

(6-BROMOHEXYL)DIETHYLAMINE HYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)CCCCCCBr.Br

Technology Process of (6-Bromohexyl)diethylamine hydrobromide

There total 1 articles about (6-Bromohexyl)diethylamine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(N,N-diethylamino)-hexanol (6947-12-2) → 6-(diethylamino)hexyl bromine hydrobromide (64993-14-2)

Guidance literature:

With hydrogen bromide; In water; at 60 - 102 ℃; for 2.5 - 3h;

Reference yield: 91.6%

8-amino-6-methoxy-4-methylquinoline (57514-21-3) + 6-(diethylamino)hexyl bromine hydrobromide (64993-14-2) + pyrographite (7440-44-0) → N,N-Diethyl-N'-(6-methoxy-4-methyl-8-quinolinyl)-1,6-hexanediamine,Dihydrochloride (5330-29-0)

Guidance literature:

With potassium hydroxide; triethylamine; In diethyl ether; water;

Reference yield:

8-amino-6-methoxy-4-methylquinoline (57514-21-3) + 6-(diethylamino)hexyl bromine hydrobromide (64993-14-2) + toluene-4-sulfonic acid (104-15-4) → N,N-diethyl-N'-[4-methyl-6-(methyloxy)-8-quinolinyl]-1,6-hexanediamine tosylate (1019640-33-5)

Guidance literature:

8-amino-6-methoxy-4-methylquinoline; 6-(diethylamino)hexyl bromine hydrobromide; With tributyl-amine; In toluene; at 101 - 115 ℃; for 5h; Heating / reflux;

With sodium hydroxide; In water; toluene; at 65 - 75 ℃; for 0.25 - 0.416667h;

toluene-4-sulfonic acid; In isopropyl alcohol; at 43 - 47 ℃; for 4h;

upstream raw materials:

6-(N,N-diethylamino)-hexanol

Downstream raw materials:

sitamaquine

N,N-Diethyl-N'-(6-methoxy-4-methyl-8-quinolinyl)-1,6-hexanediamine,Dihydrochloride

N,N-diethyl-N'-[4-methyl-6-(methyloxy)-8-quinolinyl]-1,6-hexanediamine tosylate

Refernces