3,3'-[(2-methyl-1,3-phenylene)diimino]bis[4,5,6,7-tetrachloro-1H-isoindol-1-one]

Base Information

• Chemical Name: 3,3'-[(2-methyl-1,3-phenylene)diimino]bis[4,5,6,7-tetrachloro-1H-isoindol-1-one]
• CAS No.: 5045-40-9
• Molecular Formula: C23H8Cl8N4O2
• Molecular Weight: 655.966
• Mol file: 5045-40-9.mol

Synonyms:Phthalimidine,3,3'-[(2-methyl-m-phenylene)dinitrilo]bis[4,5,6,7-tetrachloro- (6CI,7CI,8CI);Azamethine Yellow 2GLT;C.I. 56284;C.I. Pigment Yellow 109;Irgazin Yellow2GLT;Irgazin Yellow 2GLTE;Irgazin Yellow 2GLTN;Isoindolinone Yellow 2G;Isoindolinone yellow;Pigment Yellow 109;Pigment Yellow 2GLTE;UnisperseYellow 2GLT-E;4,5,6,7-tetrachloro-3-[2-methyl-3-[(4,5,6,7-tetrachloro-3-oxoisoindol-1-yl)amino]anilino]isoindol-1-one;

Chemical Property of 3,3'-[(2-methyl-1,3-phenylene)diimino]bis[4,5,6,7-tetrachloro-1H-isoindol-1-one]

Chemical Property:

• Boiling Point: 799.3 °C at 760 mmHg
• PKA: -3.70±0.20(Predicted)
• Flash Point: 437.2 °C
• PSA: 89.90000
• Density: 1.89 g/cm³
• LogP: 8.88640

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3'-[(2-methyl-1,3-phenylene)diimino]bis[4,5,6,7-tetrachloro-1H-isoindol-1-one]

There total 3 articles about 3,3'-[(2-methyl-1,3-phenylene)diimino]bis[4,5,6,7-tetrachloro-1H-isoindol-1-one] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H6Cl8N4O2(2-)*2Na(1+) → Pigment Yellow 109 (5045-40-9)

Guidance literature:

With acetic acid; In water; at 20 - 95 ℃; for 1h; Product distribution / selectivity;

Reference yield:

2,6-toluenediamine (823-40-5) + 3,4,5,6-tetrachloro-2-cyanobenzoic acid methyl ester (5358-06-5,790240-51-6) → Pigment Yellow 109 (5045-40-9)

Guidance literature:

3,4,5,6-tetrachloro-2-cyanobenzoic acid methyl ester; With sodium methylate; at 20 - 40 ℃; for 140h;

2,6-toluenediamine; In 1,2-dichloro-benzene; at 100 ℃; for 5h; Product distribution / selectivity;

Reference yield:

→ Pigment Yellow 109 (5045-40-9)

Guidance literature:

Hexachloroindoline I, 1,3-Diamino-2-methylbenzol (S.1076);

upstream raw materials:

2,6-toluenediamine

3,4,5,6-tetrachloro-2-cyanobenzoic acid methyl ester

Refernces