3-Ethylbenzenesulfonic acid sodium salt

Base Information

• Chemical Name: 3-Ethylbenzenesulfonic acid sodium salt
• CAS No.: 65130-68-9
• Molecular Formula: C₈H₉O₃S*Na
• Molecular Weight: 208.213
• Mol file: 65130-68-9.mol

Synonyms:

Chemical Property of 3-Ethylbenzenesulfonic acid sodium salt

Chemical Property:

• PSA: 65.58000
• LogP: 2.23390

Purity/Quality:

99.0%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Ethylbenzenesulfonic acid sodium salt

There total 3 articles about 3-Ethylbenzenesulfonic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Ethyl-3-trimethylsilylbenzol (17988-51-1) → Sodium; 3-ethyl-benzenesulfonate (65130-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: chlorosulfonate de trimethylsilyle / CCl₄ / 16 h / Heating

2: solution aqueuse de bicarbonate de sodium

With trimethylsilylsulfonyl chloride; solution aqueuse de bicarbonate de sodium; In tetrachloromethane;

DOI:10.1016/S0040-4020(01)81469-1

Reference yield:

2-Ethyl-1,4-bis-trimethylsilanyl-benzene (128254-32-0) → Sodium; 3-ethyl-benzenesulfonate (65130-68-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / acide trifluoroacetique / CCl₄ / 15 h / Heating

2: chlorosulfonate de trimethylsilyle / CCl₄ / 16 h / Heating

3: solution aqueuse de bicarbonate de sodium

With trimethylsilylsulfonyl chloride; acide trifluoroacetique; solution aqueuse de bicarbonate de sodium; In tetrachloromethane;

DOI:10.1016/S0040-4020(01)81469-1

Reference yield:

3-ethylbenzene-1-sulfonyl chloride (34586-44-2) → Sodium; 3-ethyl-benzenesulfonate (65130-68-9)

Guidance literature:

With solution aqueuse de bicarbonate de sodium; Yield given;

DOI:10.1016/S0040-4020(01)81469-1

upstream raw materials:

3-ethylbenzene-1-sulfonyl chloride

1-Ethyl-3-trimethylsilylbenzol

2-Ethyl-1,4-bis-trimethylsilanyl-benzene

Refernces