Decanoic acid, 10,10-dimethoxy-, methyl ester

Base Information

• Chemical Name: Decanoic acid, 10,10-dimethoxy-, methyl ester
• CAS No.: 65157-90-6
• Molecular Formula: C13H26O4
• Molecular Weight: 246.347
• Mol file: 65157-90-6.mol

Synonyms:

Chemical Property of Decanoic acid, 10,10-dimethoxy-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Decanoic acid, 10,10-dimethoxy-, methyl ester

There total 2 articles about Decanoic acid, 10,10-dimethoxy-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl 10-undecenoate (111-81-9) → methyl non-8-enoate (20731-23-1) + methyl 10,10 dimethoxy decanoate (65157-90-6)

Guidance literature:

With copper diacetate; ozone; Yield given. Multistep reaction. Yields of byproduct given; 1) light petroleum, ice bath; 2) MeOH, temp. rises to reflux, 30 min;

DOI:10.1016/S0040-4020(01)96613-X

Reference yield:

methanol (67-56-1) + Methyl 10-undecenoate (111-81-9) → dimethyl 1,18-octadecanedioate (1472-93-1) + methyl non-8-enoate (20731-23-1) + methyl 10,10 dimethoxy decanoate (65157-90-6)

Guidance literature:

With copper (I) acetate; ozone; Yield given. Multistep reaction. Yields of byproduct given; 1) MeOH; 2) MeOH;

DOI:10.1016/S0040-4020(01)96613-X

Reference yield:

methyl 10,10 dimethoxy decanoate (65157-90-6) → 10-oxo-decanoic acid methyl ester (14811-73-5)

Guidance literature:

With hydrogenchloride; In acetone; for 6h; Ambient temperature;

upstream raw materials:

methanol

Methyl 10-undecenoate

Downstream raw materials:

10-oxo-decanoic acid methyl ester

Refernces