Technology Process of 1-Azoniabicyclo[2.2.2]octane, 4-cyano-1-methyl-, iodide
There total 9 articles about 1-Azoniabicyclo[2.2.2]octane, 4-cyano-1-methyl-, iodide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phenyl sodium; benzene / Erwaermen der Reaktionsloesung
2: 260 - 270 °C / 13 Torr
3: acetone
With
phenyl sodium; acetone; benzene;
DOI:10.1002/hlca.19540370610
- Guidance literature:
-
Multi-step reaction with 5 steps
1: methanol / Hydrieren des Reaktionsgemisches an Raney-Nickel
2: SOCl2; benzene
3: phenyl sodium; benzene / Erwaermen der Reaktionsloesung
4: 260 - 270 °C / 13 Torr
5: acetone
With
methanol; thionyl chloride; phenyl sodium; acetone; benzene;
DOI:10.1002/hlca.19540370610
- Guidance literature:
-
Multi-step reaction with 7 steps
1: acetone
2: Raney nickel; methanol; triethylamine / 90 °C / 73550.8 Torr / Hydrogenation
3: NH3; methanol
4: SOCl2; benzene
5: phenyl sodium; benzene / Erwaermen der Reaktionsloesung
6: 260 - 270 °C / 13 Torr
7: acetone
With
methanol; thionyl chloride; ammonia; phenyl sodium; nickel; triethylamine; acetone; benzene;
DOI:10.1002/hlca.19540370610