Technology Process of (NZ)-N-[(4-phenylphenyl)methylidene]hydroxylamine
There total 4 articles about (NZ)-N-[(4-phenylphenyl)methylidene]hydroxylamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium carbonate;
In
methanol; water;
at 20 ℃;
for 3h;
DOI:10.1039/c6ra02222g
- Guidance literature:
-
4-bromo-1,1'-biphenyl;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -50 ℃;
for 0.5h;
Inert atmosphere;
N,N-dimethyl-formamide;
In
tetrahydrofuran; hexane;
at -50 - 20 ℃;
for 1h;
Inert atmosphere;
With
hydroxylamine hydrochloride; potassium carbonate;
In
tetrahydrofuran; hexane;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1016/j.tet.2018.06.044
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium chlorochromate; magnesium sulfate / chloroform / 3 h / Sealed tube
2: hydroxylamine hydrochloride; sodium acetate / water; ethanol; tetrahydrofuran / 72 h / 20 °C
With
hydroxylamine hydrochloride; sodium acetate; magnesium sulfate; pyridinium chlorochromate;
In
tetrahydrofuran; ethanol; chloroform; water;
DOI:10.1016/j.tetlet.2015.12.038
