Benz[a]anthracen-7-amine

Base Information

• Chemical Name: Benz[a]anthracen-7-amine
• CAS No.: 2381-18-2
• Molecular Formula: C₁₈H₁₃N
• Molecular Weight: 243.308
• Hs Code.: 2921199090
• Mol file: 2381-18-2.mol

Synonyms:7-Aminobenz[a]anthracene

Chemical Property of Benz[a]anthracen-7-amine

Chemical Property:

• Vapor Pressure: 5.79E-10mmHg at 25°C
• Melting Point: 175°C
• Refractive Index: 1.4500 (estimate)
• Boiling Point: 495.7°Cat760mmHg
• Flash Point: 282.7°C
• PSA: 26.02000
• Density: 1.253g/cm³
• LogP: 5.30960

Purity/Quality:

99% ^*data from raw suppliers

7-AMINOBENZ[A]ANTHRACENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benz[a]anthracen-7-amine

There total 4 articles about Benz[a]anthracen-7-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

7-nitrobenz[a]anthracene (20268-51-3) → 7-aminobenzanthracene (2381-18-2)

Guidance literature:

With ammonium acetate; zinc; In water; Product distribution; Ambient temperature; influence of ammonium acetate; the lenght of the reducer column;;

DOI:10.1021/ac00154a001

Reference yield:

hydroxy-benzanthracene (28186-96-1) → 7-aminobenzanthracene (2381-18-2)

Guidance literature:

With 1,4-dioxane; ammonium hydroxide; sodium hydrogensulfite;

DOI:10.1021/ja01275a047

Reference yield:

→ 7-aminobenzanthracene (2381-18-2)

Guidance literature:

With sodium azide; chloroform; sulfuric acid; at 40 - 50 ℃;

DOI:10.1039/jr9490000799

upstream raw materials:

7-nitrobenz[a]anthracene

hydroxy-benzanthracene

ethyl acetate

Downstream raw materials:

7-Fluorobenzoanthracene

Refernces