2,4,6-Cycloheptatrien-1-one, 5-[5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3-dihydro-1,4-benzo dioxin-6-yl]-2-methoxy-

Base Information

• Chemical Name: 2,4,6-Cycloheptatrien-1-one, 5-[5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3-dihydro-1,4-benzo dioxin-6-yl]-2-methoxy-
• CAS No.: 669051-38-1
• Molecular Formula: C23H30O5Si
• Molecular Weight: 414.574
• Mol file: 669051-38-1.mol

Synonyms:

Chemical Property of 2,4,6-Cycloheptatrien-1-one, 5-[5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3-dihydro-1,4-benzo dioxin-6-yl]-2-methoxy-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,6-Cycloheptatrien-1-one, 5-[5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3-dihydro-1,4-benzo dioxin-6-yl]-2-methoxy-

There total 1 articles about 2,4,6-Cycloheptatrien-1-one, 5-[5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-2,3-dihydro-1,4-benzo dioxin-6-yl]-2-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-bromo-2-methoxycyclohepta-2,4,6-trien-1-one (33816-51-2) + C15H25BO5Si → 2-methoxy-5-{5-[(1,1,2,2-tetramethyl-1-silapropoxy)methyl](2H,3H-benzo[e]1,4-dioxin-6-yl)}cyclohepta-2,4,6-trien-1-one (669051-38-1)

Guidance literature:

With palladium diacetate; tetrabutylammomium bromide; potassium carbonate; In water; at 70 ℃;

DOI:10.1016/j.tetlet.2003.11.016

upstream raw materials:

5-bromo-2-methoxycyclohepta-2,4,6-trien-1-one

Refernces