Technology Process of Lead(II) thiocyanate
There total 26 articles about Lead(II) thiocyanate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
water;
addn. of 1M aq. Pb(NO3)2 soln. to 136ml 10M NH4SCN soln. at 5°C, stirring for 30min; (exclusion of light);; washing with H2O of 5°C, drying in vac. over P2O5 for about 8d; (exclusion of light);;
- Guidance literature:
-
In
water;
addn. of 90g KSCN in 840ml H2O to 150g Pb(NO3)2 in 1500ml H2O at ambient temp. while stirring, cooling, crystn.;; filtration in the cold, washing with ice-cooled H2O, drying on clay in the dark; yield: 90g;;