N-(2,4-Dinitrophenyl)ethanehydrazonoyl bromide

Base Information

• Chemical Name: N-(2,4-Dinitrophenyl)ethanehydrazonoyl bromide
• CAS No.: 15009-34-4
• Molecular Formula: C₈H₇BrN₄O₄
• Molecular Weight: 303.072
• Mol file: 15009-34-4.mol

Synonyms:N-(2,4-Dinitrophenyl)ethanehydrazonoyl bromide;15009-34-4;ACETYL BROMIDE, 2,4-DINITROPHENYLHYDRAZONE;BRN 0673853;Ethanehydrazonoyl bromide, N-(2,4-dinitrophenyl)-;(1Z)-N-(2,4-dinitrophenyl)ethanehydrazonoyl bromide

Chemical Property of N-(2,4-Dinitrophenyl)ethanehydrazonoyl bromide

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 149-150 °C
• Boiling Point: 402.2°Cat760mmHg
• PKA: 13?+-.0.10(Predicted)
• Flash Point: 197°C
• PSA: 116.03000
• Density: 1.83g/cm³
• LogP: 3.76260
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 2
• Exact Mass: 301.96507
• Heavy Atom Count: 17
• Complexity: 337

Purity/Quality:

N-(2,4-DINITROPHENYL)ETHANEHYDRAZONOYL BROMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(=NNC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-])Br
• Isomeric SMILES: C/C(=N/NC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-])/Br

Technology Process of N-(2,4-Dinitrophenyl)ethanehydrazonoyl bromide

There total 1 articles about N-(2,4-Dinitrophenyl)ethanehydrazonoyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ C8H7BrN4O4 (15009-34-4)

Guidance literature:

entspr. 'Phenylhydrazon', Br2;

Reference yield: 20.0%

5-methoxy-1H-tetrazole (5376-15-8) + C8H7BrN4O4 (15009-34-4) → N-(2,4-Dinitro-phenyl)-N'-[1-(5-methoxy-tetrazol-2-yl)-eth-(Z)-ylidene]-hydrazine (114065-23-5) + N-(2,4-Dinitro-phenyl)-N'-[1-(5-methoxy-tetrazol-1-yl)-eth-(Z)-ylidene]-hydrazine (114064-71-0)

Guidance literature:

With triethylamine; In ethanol; for 1h; Ambient temperature;

Reference yield:

C8H7BrN4O4 (15009-34-4) → acetic acid-[N'-(2,4-dinitro-phenyl)-hydrazide] (2719-07-5)

Guidance literature:

With water; In acetone;

DOI:10.1021/jo01266a055

Downstream raw materials:

acetic acid-[N'-(2,4-dinitro-phenyl)-hydrazide]

N-(2,4-Dinitro-phenyl)-N'-[1-(5-methoxy-tetrazol-2-yl)-eth-(Z)-ylidene]-hydrazine

N-(2,4-Dinitro-phenyl)-N'-[1-(5-methoxy-tetrazol-1-yl)-eth-(Z)-ylidene]-hydrazine

1-(2,4-Dinitro-phenyl)-5-methoxy-3-methyl-1H-[1,2,4]triazole