Phenol, 3,3'-[1,2-ethanediylbis(oxy)]bis-

Base Information

• Chemical Name: Phenol, 3,3'-[1,2-ethanediylbis(oxy)]bis-
• CAS No.: 61166-00-5
• Molecular Formula: C14H14O4
• Molecular Weight: 246.263
• Hs Code.: 2909500000
• European Community (EC) Number: 262-630-4
• DSSTox Substance ID: DTXSID6069458
• Nikkaji Number: J193.338H
• Wikidata: Q72474737
• Mol file: 61166-00-5.mol

Synonyms:61166-00-5;3,3'-Ethylenedioxydiphenol;3,3'-(Ethane-1,2-diylbis(oxy))diphenol;1,2-Bis(3-hydroxyphenoxy)ethane;Phenol, 3,3'-[1,2-ethanediylbis(oxy)]bis-;3-[2-(3-hydroxyphenoxy)ethoxy]phenol;EINECS 262-630-4;Phenol, 3,3'-(1,2-ethanediylbis(oxy))bis-;3,3'-(1,2-Ethanediylbis(oxy))bisphenol;3,3'-[1,2-ethanediylbis(oxy)]bisphenol;3,3'-[ethane-1,2-diylbis(oxy)]diphenol;Bisresorcine ethylene ether;SCHEMBL1470185;DTXSID6069458;MFCD00002268;AKOS015840287;Ethylene Glycol Bis(3-hydroxyphenyl) Ether;CS-0454107;E0448;FT-0720706;3,3'-(Ethylenedioxy)diphenol, 85%, technical grade

Chemical Property of Phenol, 3,3'-[1,2-ethanediylbis(oxy)]bis-

Chemical Property:

• Melting Point: 157-160 °C(lit.)
• Boiling Point: 466.6 °C at 760 mmHg
• Flash Point: 236 °C
• PSA: 58.92000
• Density: 1.261 g/cm³
• LogP: 2.55560
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 246.08920892
• Heavy Atom Count: 18
• Complexity: 210

Purity/Quality:

98%,99%, ^*data from raw suppliers

3,3′-(Ethylenedioxy)diphenol 85%, technical grade ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)OCCOC2=CC=CC(=C2)O)O

Technology Process of Phenol, 3,3'-[1,2-ethanediylbis(oxy)]bis-

There total 2 articles about Phenol, 3,3'-[1,2-ethanediylbis(oxy)]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethylene dibromide (106-93-4) + recorcinol (108-46-3) → 1,4-bis(3-hydroxyphenyl)-1,4-dioxabutane (61166-00-5)

Guidance literature:

With potassium hydroxide;

Reference yield:

→ 1,4-bis(3-hydroxyphenyl)-1,4-dioxabutane (61166-00-5)

Guidance literature:

resorcinol (1c), ethylene chloride, KOH, in DMSO, under N2;

Reference yield: 74.0%

1,4-bis(3-hydroxyphenyl)-1,4-dioxabutane (61166-00-5) + ethyl 3-oxo-3-phenylpropionate (94-02-0) → 4,4'-diphenyl-7,7'-ethane-1,2-diyldioxy-bis-chromen-2-one (66346-12-1)

Guidance literature:

With perchloric acid; at 75 - 80 ℃;

DOI:10.1002/jhet.5570430501

upstream raw materials:

ethylene dibromide

recorcinol

Downstream raw materials:

1,2-C₂H₄(O-3-C₆H₄OCH₂CCH)2

4,4'-diphenyl-7,7'-ethane-1,2-diyldioxy-bis-chromen-2-one