Iron, bis(3-methylbenzenamine)(ethanedioato(2-)-O,O')-

Base Information

• Chemical Name: Iron, bis(3-methylbenzenamine)(ethanedioato(2-)-O,O')-
• CAS No.: 74910-19-3
• Molecular Formula: C₁₆H₁₈FeN₂O₄
• Molecular Weight: 358.177
• DSSTox Substance ID: DTXSID70225889
• Mol file: 74910-19-3.mol

Synonyms:Iron, bis(3-methylbenzenamine)(ethanedioato(2-)-O,O')-;Iron, (ethanedioato(2-)-O,O')bis(3-methylbenzenamine)-;74910-19-3;C16H18N2O4.Fe;DTXSID70225889;C16-H18-N2-O4.Fe;LS-84225

Chemical Property of Iron, bis(3-methylbenzenamine)(ethanedioato(2-)-O,O')-

Chemical Property:

• Vapor Pressure: 0.278mmHg at 25°C
• Boiling Point: 203.4°C at 760 mmHg
• Flash Point: 85.6°C
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 0
• Exact Mass: 358.061593
• Heavy Atom Count: 23
• Complexity: 131

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=CC=C1)N.CC1=CC(=CC=C1)N.C(=O)(C(=O)[O-])[O-].[Fe+2]

Technology Process of Iron, bis(3-methylbenzenamine)(ethanedioato(2-)-O,O')-

There total 1 articles about Iron, bis(3-methylbenzenamine)(ethanedioato(2-)-O,O')- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iron(II) oxalate dihydrate (6047-25-2) + 1-amino-3-methylbenzene (108-44-1) → Fe(CH3C6H4NH2)2C2O4 (74910-19-3)

Guidance literature:

In ethanol; excess of ligand was added to ethanolic suspn. of iron(II) oxalate, shaking for 5-6 h, mixt. was allowed to stand for another 6 h; filtered, washed with dry ether and finally dried in vac. desiccator over CaCl2, elem. anal.;

upstream raw materials:

iron(II) oxalate dihydrate

1-amino-3-methylbenzene

Refernces