Valine, 3,3'-dithiobis[N-acetyl-

Base Information

• Chemical Name: Valine, 3,3'-dithiobis[N-acetyl-
• CAS No.: 67809-84-1
• Molecular Formula: C14H24N2O6S2
• Molecular Weight: 380.486
• Mol file: 67809-84-1.mol

Synonyms:Valine,3,3'-dithiobis[N-acetyl;

Chemical Property of Valine, 3,3'-dithiobis[N-acetyl-

Chemical Property:

• PSA: 190.38000
• LogP: 2.78420

Purity/Quality:

99% ^*data from raw suppliers

3,3'-Dithiobis[(R)-2-(acetylamino)-3-methylbutyric acid] 95+% ee ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Valine, 3,3'-dithiobis[N-acetyl-

There total 4 articles about Valine, 3,3'-dithiobis[N-acetyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

S-nitroso-N-acetyl-DL-penicillamine (67776-06-1,81739-40-4) → NAP (59-53-0) + N-acetyl-D,L-penicillamine disulfide (67809-84-1)

Guidance literature:

With ethylenediaminetetraacetic acid; buffer reagents; ascorbic acid; In water; Further Variations:; Reagents; Kinetics;

Reference yield:

S-nitroso-N-acetyl-DL-penicillamine (67776-06-1,81739-40-4) → N-acetyl-D,L-penicillamine disulfide (67809-84-1)

Guidance literature:

With copper(II) ion; In water; other metal cations; also in the presence of EDTA or amine; catalysed decomposition reaction;

DOI:10.1039/c39930001758

Reference yield:

pentacyanonitrosylferrate(III) + NAP (59-53-0) → N-acetyl-D,L-penicillamine disulfide (67809-84-1) + hexacyanoferrate(II)

Guidance literature:

In water; Kinetics;

DOI:10.1016/S0277-5387(00)81208-5

upstream raw materials:

S-nitroso-N-acetyl-DL-penicillamine

NAP

Refernces

• 1、 Zhou, Yang,Tan, Jinyi,Dai, Yuping,Yu, Yanmin,Zhang, Qi,Meyerhoff, Mark E.. "Synthesis and nitric oxide releasing properties of novel fluoro S-nitrosothiols". supporting information. p. 401 - 404. Retrieved 2019/01/09.
• 2、 Williams, D. Lyn H.. "The mechanism of nitric oxide formation from S-nitrosothiols (thionitrites)". . p. 1085 - 1091. Retrieved 2007/10/03.