Technology Process of 5H-Dibenzo[b,e]azepine-6,11-dione
There total 13 articles about 5H-Dibenzo[b,e]azepine-6,11-dione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide; sulfuric acid;
In
dichloromethane;
at 0 - 20 ℃;
- Guidance literature:
-
With
trimethylsilylazide; diphenyl phosphoryl azide; water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride;
In
trifluoroacetic acid;
at 100 ℃;
for 96h;
Inert atmosphere;
DOI:10.1002/anie.201106112