2-Butenoic acid, 2-fluoro-3-methyl-, ethyl ester

Base Information Edit

Chemical Name:2-Butenoic acid, 2-fluoro-3-methyl-, ethyl ester
CAS No.:685-89-2
Molecular Formula:C₇H₁₁FO₂
Molecular Weight:146.162
Hs Code.:
DSSTox Substance ID:DTXSID401238909
Nikkaji Number:J721.755B
Mol file:685-89-2.mol

Synonyms:685-89-2;2-Butenoic acid, 2-fluoro-3-methyl-, ethyl ester;ethyl 2-fluoro-3-methylbut-2-enoate;2-fluoro-3-methyl-but-2-enoic acid ethyl ester;SCHEMBL3365717;BNWNCVHANYORFN-UHFFFAOYSA-N;DTXSID401238909;ethyl2-fluoro-3-methylbut-2-enoate;AKOS028112318;2-Fluoro-3-methyl-2-butenoic acid ethyl ester;EN300-205074

Suppliers and Price of 2-Butenoic acid, 2-fluoro-3-methyl-, ethyl ester

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
ethyl2-fluoro-3-methylbut-2-enoate
50mg
$ 200.00

AHH
methyl2-bromo-6-chlorobenzoate 97%
5g
$ 595.00

Total 6 raw suppliers

Chemical Property of 2-Butenoic acid, 2-fluoro-3-methyl-, ethyl ester Edit

Chemical Property:

Vapor Pressure:0.00538mmHg at 25°C
Melting Point:54-56°C
Boiling Point:274.5oC at 760 mmHg
Flash Point:119.8oC
PSA：26.30000
Density:1.604g/cm3
LogP:2.88910
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:146.07430775
Heavy Atom Count:10
Complexity:157

Purity/Quality:

98% ^*data from raw suppliers

ethyl2-fluoro-3-methylbut-2-enoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=C(C)C)F

Technology Process of 2-Butenoic acid, 2-fluoro-3-methyl-, ethyl ester

There total 9 articles about 2-Butenoic acid, 2-fluoro-3-methyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.1%

: 2356-16-3
ethyl(diethylphosphono)(fluoro)acetate

: 67-64-1
acetone

: 685-89-2
ethyl 2-fluoro-3-methyl-but-2-en-oate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -70 - 20 ℃; Inert atmosphere;

Reference yield: 61.6%

: 67-64-1
acetone

: 685-89-2
ethyl 2-fluoro-3-methyl-but-2-en-oate

Guidance literature:: ethyl(diethylphosphono)(fluoro)acetate; With sodium hydride; In 1,2-dimethoxyethane; at 0 - 20 ℃; for 0.333333h;

acetone; In metthoxyethane; Heating / reflux;

Reference yield: 44.7%

: C₈H₁₆FO₄P

: 67-64-1
acetone

: 685-89-2
ethyl 2-fluoro-3-methyl-but-2-en-oate

Guidance literature:: C₈H₁₆FO₄P; With sodium hydride; In 1,2-dimethoxyethane; at 0 - 20 ℃; for 1h; Inert atmosphere;

acetone; In 1,2-dimethoxyethane; at 90 ℃; for 16h; Inert atmosphere;