carbazol-9-yl-pyridin-3-yl-methanone

Base Information

• Chemical Name: carbazol-9-yl-pyridin-3-yl-methanone
• CAS No.: 7469-85-4
• Molecular Formula: C₁₈H₁₂N₂O
• Molecular Weight: 272.306
• Mol file: 7469-85-4.mol

Synonyms:9H-Carbazole,9-(3-pyridinylcarbonyl)- (9CI); NSC 402301

Chemical Property of carbazol-9-yl-pyridin-3-yl-methanone

Chemical Property:

• Vapor Pressure: 5.62E-07mmHg at 25°C
• Boiling Point: 411.4°C at 760 mmHg
• Flash Point: 202.6°C
• PSA: 34.89000
• Density: 1.23g/cm³
• LogP: 3.87800

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of carbazol-9-yl-pyridin-3-yl-methanone

There total 22 articles about carbazol-9-yl-pyridin-3-yl-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-(2-chloro-3-pyridinecarbonyl)carbazole (866594-42-5) → 9-(3-pyridinecarbonyl)carbazole (7469-85-4) + 8H-[1,6]naphthyridino[8,7,6-jk]carbazol-8-one + 9H-carbazole (86-74-8,105184-46-1,97960-57-1)

Guidance literature:

With tri-n-butyl-tin hydride; 1,1'-azobis(1-cyanocyclohexanenitrile); In toluene; Heating;

DOI:10.1016/j.tet.2005.07.034

Reference yield:

9-(4-bromo-3-pyridinecarbonyl)carbazole (866594-50-5) → 9-(3-pyridinecarbonyl)carbazole (7469-85-4) + 8H-[2,7]naphthyridino[4,3,2-jk]carbazol-8-one + 9H-carbazole (86-74-8,105184-46-1,97960-57-1)

Guidance literature:

With tri-n-butyl-tin hydride; 1,1'-azobis(1-cyanocyclohexanenitrile); In toluene; Heating;

DOI:10.1016/j.tet.2005.07.034

Reference yield:

9-(4-chloro-3-pyridinecarbonyl)carbazole (866594-44-7) → 9-(3-pyridinecarbonyl)carbazole (7469-85-4) + 8H-[2,7]naphthyridino[4,3,2-jk]carbazol-8-one + 9H-carbazole (86-74-8,105184-46-1,97960-57-1)

Guidance literature:

With tri-n-butyl-tin hydride; 1,1'-azobis(1-cyanocyclohexanenitrile); In toluene; Heating;

DOI:10.1016/j.tet.2005.07.034

upstream raw materials:

9-(2-chloro-3-pyridinecarbonyl)carbazole

9-(2-bromo-3-pyridinecarbonyl)carbazole

9-(4-bromo-3-pyridinecarbonyl)carbazole

9-(4-chloro-3-pyridinecarbonyl)carbazole

Refernces