Dicyclohexylamine nitrite

Base Information

• Chemical Name: Dicyclohexylamine nitrite
• CAS No.: 3129-91-7
• Molecular Formula: C12H23N^.HNO2
• Molecular Weight: 228.335
• Hs Code.: Oral rat LD50: 330 mg/kg
• European Community (EC) Number: 221-515-9
• NSC Number: 49612
• UN Number: 2687
• UNII: D39V3CN62U
• Wikidata: Q26840917
• Mol file: 3129-91-7.mol

Synonyms:cyclohexanamine, N-cyclohexyl-, sulfate (1:1);dicyclohexylamine;dicyclohexylamine hydrochloride;dicyclohexylamine nitrate;dicyclohexylamine nitrite;dicyclohexylamine phosphate (3:1);dicyclohexylamine sulfate;dicyclohexylamine sulfate (1:1);dicyclohexylammonium

Chemical Property of Dicyclohexylamine nitrite

Chemical Property:

• Appearance/Colour: white powder
• Vapor Pressure: 3.3 mm Hg ( 25 °C)
• Melting Point: 182 - 183 C (Decomposes)
• Refractive Index: 1.4560 (estimate)
• Boiling Point: 256.1°Cat760mmHg
• Flash Point: 100 C
• PSA: 61.69000
• Density: 0.91g/cm³
• LogP: 3.77430
• Storage Temp.: 2-8°C
• Water Solubility.: Soluble in water
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 228.183778013
• Heavy Atom Count: 16
• Complexity: 126
• Transport DOT Label: Flammable Solid

Purity/Quality:

99% ^*data from raw suppliers

DicyclohexylammoniumNitrite ^*data from reagent suppliers

Safty Information:

• Pictogram(s): 4.1 (Packing Group: III) UN NO.
• Hazard Codes: Xn
• Statements: 20/22
• Safety Statements: 15-41

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Nitrogen Compounds -> Amines, Cyclic
• Canonical SMILES: C1CCC(CC1)NC2CCCCC2.N(=O)O

Technology Process of Dicyclohexylamine nitrite

There total 1 articles about Dicyclohexylamine nitrite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ dicyclohexylamine nitrite (3129-91-7)

Guidance literature:

Herstellung von Bis-<1-¹⁴C>cyclohexyl-ammonium-nitrit;

DOI:10.1021/jo01115a601

Reference yield: 1.06%

dicyclohexylamine x nitrite (3129-91-7) → N-nitrosodicyclohexylamine (947-92-2)

Guidance literature:

With sodium nitrite; In sulfuric acid; for 2h;

DOI:10.1007/s002040000205

Reference yield:

dicyclohexylamine nitrite (3129-91-7) → acetic acid (64-19-7,77671-22-8) + propionic acid (802294-64-0,79-09-4) + isobutyric Acid (79-31-2) + butyric acid (107-92-6) + valeric acid (109-52-4)

Guidance literature:

With ozone; In water; at 40 ℃; for 1.16667h; Product distribution; diff. concentrations of O₃; diff. reaction time; influence of alkaline;

Downstream raw materials:

acetic acid

propionic acid

isobutyric Acid

butyric acid