Decanoic acid, 2-oxo-1,3-propanediyl ester

Base Information

• Chemical Name: Decanoic acid, 2-oxo-1,3-propanediyl ester
• CAS No.: 73312-67-1
• Molecular Formula: C23H42O5
• Molecular Weight: 398.583
• Mol file: 73312-67-1.mol

Synonyms:

Chemical Property of Decanoic acid, 2-oxo-1,3-propanediyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Decanoic acid, 2-oxo-1,3-propanediyl ester

There total 1 articles about Decanoic acid, 2-oxo-1,3-propanediyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1,3-dihydroxyacetone dimer (62147-49-3) + n-decanoyl chloride (112-13-0) → 1,3-dicaproyloxypropan-2-one (73312-67-1) + pyridine hydrochloride (628-13-7)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 20 - 30 ℃;

Reference yield: 100.0%

1,3-dicaproyloxypropan-2-one (73312-67-1) → 1, 3-dicaprin (17598-93-5)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; at 0 - 20 ℃; for 0.25h;

Reference yield:

1,3-dicaproyloxypropan-2-one (73312-67-1) → 2-(3-Trifluoromethyl-phenylamino)-nicotinic acid 2-decanoyloxy-1-decanoyloxymethyl-ethyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: NaBH₄

2: 92 percent / allyl bromide, CDI / 16 h / Heating

With sodium tetrahydroborate; allyl bromide; 1,1'-carbonyldiimidazole;

upstream raw materials:

1,3-dihydroxyacetone dimer

n-decanoyl chloride

Downstream raw materials:

1, 3-dicaprin

Refernces