CID 53817926

Base Information Edit

Chemical Name:CID 53817926
CAS No.:7386-61-0
Molecular Formula:C11H9F3O2
Molecular Weight:230.186
Hs Code.:
DSSTox Substance ID:DTXSID40706897
Mol file:7386-61-0.mol

Synonyms:7386-61-0;DTXSID40706897;AKOS016904620

Suppliers and Price of CID 53817926

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of CID 53817926 Edit

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:230.05546401
Heavy Atom Count:16
Complexity:286

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CC(=O)O)C1=CC=C(C=C1)C(F)(F)F

Technology Process of CID 53817926

There total 5 articles about CID 53817926 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 581812-94-4
(E)-ethyl 3-(4-(trifluoromethyl)phenyl)but-2-enoate

: 7386-61-0
(E)-3-(4-(trifluoromethyl)phenyl)but- 2-enoic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; at 20 ℃; for 16h;
DOI:10.1021/jacs.5b12081

Reference yield: 53.0%

: 124-38-9,18923-20-1
carbon dioxide

: 705-31-7
4-trifluoromethylphenylacetylene

: 544-97-8
dimethyl zinc(II)

: 7386-61-0
(E)-3-(4-(trifluoromethyl)phenyl)but- 2-enoic acid

Guidance literature:: carbon dioxide; 4-trifluoromethylphenylacetylene; With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 0 ℃; for 1h;

dimethyl zinc(II); In tetrahydrofuran; hexane; at 0 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; hexane; Further stages.;
DOI:10.1021/ol016585z