5,10-dihydro-5-methylphenazine

Base Information

• Chemical Name: 5,10-dihydro-5-methylphenazine
• CAS No.: 20057-16-3
• Molecular Formula: C13H12N2
• Molecular Weight: 196.252
• Hs Code.: 2933990090
• Mol file: 20057-16-3.mol

Synonyms:5-methyl-5,10-dihydrophnazine;5-Methyl-5,10-dihydro-phenazin;fully reduced 5-methylphenazinium;N-methyl-N'-hydrophenazine;5-methyl-5,10-dihydro-phenazine;5,10-Dihydro-5-methylphenazine;5,10-Dihydro-5-methyl-phenazin;Phenazine,5,10-dihydro-5-methyl;

Chemical Property of 5,10-dihydro-5-methylphenazine

Chemical Property:

• Vapor Pressure: 5.72E-05mmHg at 25°C
• Melting Point: 164-165 °C
• Boiling Point: 346.5°Cat760mmHg
• PKA: 6.25±0.20(Predicted)
• Flash Point: 169.6°C
• PSA: 20.72000
• Density: 1.133g/cm³
• LogP: 3.22180

Purity/Quality:

5,10-dihydro-5-methyl-Phenazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 5,10-dihydro-5-methyl-Phenazine is a compound used frequently in electron-transfer reaction analyses.

Technology Process of 5,10-dihydro-5-methylphenazine

There total 14 articles about 5,10-dihydro-5-methylphenazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

Phenazin (92-82-0) + dimethyl sulfate (77-78-1) → fully reduced 5-methylphenazinium (20057-16-3,63631-49-2)

Guidance literature:

Phenazin; dimethyl sulfate; In nitrobenzene; at 100 ℃; for 0.116667h;

With sodium dithionite; In ethanol;

Reference yield: 94.0%

phenazine methosulfate (299-11-6) → fully reduced 5-methylphenazinium (20057-16-3,63631-49-2)

Guidance literature:

With sodium dithionite; In ethanol;

DOI:10.1002/jhet.5570360437

Reference yield: 92.0%

5,10-dihydrophenazine (613-32-1) + methyl iodide (74-88-4) → fully reduced 5-methylphenazinium (20057-16-3,63631-49-2)

Guidance literature:

5,10-dihydrophenazine; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h;

methyl iodide; With phosphorus; In tetrahydrofuran; at 66 ℃; for 4h;

upstream raw materials:

5,10-dihydrophenazine

methyl iodide

5-methylphenazinium

10-methyl-5(10H)-phenazinyl

Downstream raw materials:

10-methyl-2(10H)-phenathiazineone

Phenazin

5-(3,5-Dinitro-benzyl)-10-methyl-5,10-dihydro-phenazine; compound with 2-(4-dicyanomethylene-cyclohexa-2,5-dienylidene)-malononitrile

5-Methyl-10-(4-nitro-benzyl)-5,10-dihydro-phenazine; compound with 2-(4-dicyanomethylene-cyclohexa-2,5-dienylidene)-malononitrile

Refernces

• 1、 -. "HETEROAROMATIC DERIVATIVE COMPOUND FOR ORGANIC ELECTROLUMINESCENT DEVICE AND ORGANIC ELECTROLUMINESCENT DEVICE COMPRISING THE SAME". Paragraph 0201-0205. . Retrieved 2020/12/30.
• 2、 -. "Compounds having cGMP-PDE inhibitory effect". . . Retrieved 2008/06/13.