Technology Process of 9,10-Anthracenedione, 2,3-bis(2-chloro-2-propenyl)-1,4-dihydroxy-
There total 1 articles about 9,10-Anthracenedione, 2,3-bis(2-chloro-2-propenyl)-1,4-dihydroxy- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
1,2-dichloro-benzene;
at 180 ℃;
for 40h;
Product distribution;
Mechanism;
other substituted anthraquinones, other solvent, other time;
DOI:10.1071/CH9810819
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 88 percent / KOH / ethanol / 2.5 h / Heating
2: 4 percent / O3, pyridine / CH2Cl2 / 2 h / -78 - 20 °C
3: 92 percent / K2CO3, KI / acetone / 48 h / Heating
4: 99 percent / sodium dithionite / dimethylformamide; H2O / 0.25 h / Heating
5: 70 percent / 50 percent aq. KOH, tetrabutylammonium bromide / CH2Cl2; H2O / 21 h
With
pyridine; potassium hydroxide; sodium dithionite; tetrabutylammomium bromide; potassium carbonate; ozone; potassium iodide;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 88 percent / KOH / ethanol / 2.5 h / Heating
2: 4 percent / O3, pyridine / CH2Cl2 / 2 h / -78 - 20 °C
3: 92 percent / K2CO3, KI / acetone / 48 h / Heating
4: 99 percent / sodium dithionite / dimethylformamide; H2O / 0.25 h / Heating
5: 83 percent / 10 percent aq. KOH, tetrabutylammonium bromide / CH2Cl2 / 18 h / Ambient temperature
With
pyridine; potassium hydroxide; sodium dithionite; tetrabutylammomium bromide; potassium carbonate; ozone; potassium iodide;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;