Technology Process of Benzene, 1,4-dichloro-2-(chloromethyl)-5-[(octylsulfinyl)methyl]-
There total 4 articles about Benzene, 1,4-dichloro-2-(chloromethyl)-5-[(octylsulfinyl)methyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 36 percent / N-bromosuccinimide; dibenzoyl peroxide / benzene / 24 h / Heating; irradiation
2: 94 percent / LiCl / acetone / 24 h / Heating
3: NaOH / Aliquat 336 / toluene; H2O / 5 h
4: 600 mg / H2O2; TeO2; aq. HCl / dioxane
With
hydrogenchloride; tellurium oxide; sodium hydroxide; N-Bromosuccinimide; dihydrogen peroxide; lithium chloride; dibenzoyl peroxide;
Aliquat 336;
In
1,4-dioxane; water; acetone; toluene; benzene;
DOI:10.1002/mrc.1455
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaOH / Aliquat 336 / toluene; H2O / 5 h
2: 600 mg / H2O2; TeO2; aq. HCl / dioxane
With
hydrogenchloride; tellurium oxide; sodium hydroxide; dihydrogen peroxide;
Aliquat 336;
In
1,4-dioxane; water; toluene;
DOI:10.1002/mrc.1455
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 94 percent / LiCl / acetone / 24 h / Heating
2: NaOH / Aliquat 336 / toluene; H2O / 5 h
3: 600 mg / H2O2; TeO2; aq. HCl / dioxane
With
hydrogenchloride; tellurium oxide; sodium hydroxide; dihydrogen peroxide; lithium chloride;
Aliquat 336;
In
1,4-dioxane; water; acetone; toluene;
DOI:10.1002/mrc.1455