Technology Process of 1,2-Propanediol, 3-(octadecyloxy)-, 1-acetate, (S)-
There total 23 articles about 1,2-Propanediol, 3-(octadecyloxy)-, 1-acetate, (S)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: toluene / 1 h / 80 °C
2: pyridine / CHCl3 / Ambient temperature
3: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature
4: phosphorus oxychloride, Et3N, pyridine / CHCl3 / Ambient temperature
5: 66 percent / LiAlH4 / tetrahydrofuran / Ambient temperature
6: 81 percent / pyridine / Ambient temperature
7: NaH / dimethylformamide / 80 °C
8: 1N HCl / dioxane / 90 °C
9: pyridine / CHCl3 / Ambient temperature
10: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature
With
pyridine; hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium hydride; triethylamine; trichlorophosphate;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.19820650339
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 81 percent / pyridine / Ambient temperature
2: NaH / dimethylformamide / 80 °C
3: 1N HCl / dioxane / 90 °C
4: pyridine / CHCl3 / Ambient temperature
5: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature
With
pyridine; hydrogenchloride; hydrogen; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19820650339
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 87 percent / NaH / dimethylformamide; petroleum ether / 3 h / 50 °C
2: 81.5 percent / 1N HCl / dioxane / 1 h / Heating
3: 81 percent / pyridine / Ambient temperature
4: NaH / dimethylformamide / 80 °C
5: 1N HCl / dioxane / 90 °C
6: pyridine / CHCl3 / Ambient temperature
7: H2 / 5percent Pd/C / tetrahydrofuran / Ambient temperature
With
pyridine; hydrogenchloride; hydrogen; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; chloroform; N,N-dimethyl-formamide; Petroleum ether;
DOI:10.1002/hlca.19820650339