Phenanthrene, 9-dodecyltetradecahydro-

Base Information

• Chemical Name: Phenanthrene, 9-dodecyltetradecahydro-
• CAS No.: 55334-01-5
• Molecular Formula: C26H48
• Molecular Weight: 360.6593
• Hs Code.: 2902199090
• NSC Number: 166267
• DSSTox Substance ID: DTXSID20304552
• Nikkaji Number: J129.569A
• Mol file: 55334-01-5.mol

Synonyms:Phenanthrene, 9-dodecyltetradecahydro-;55334-01-5;9-n-Dodecylperhydrophenanthrene;9-n-Dodecyl(tetradecahydrophenanthrene);9-n-Dodecyl[tetradecahydrophenanthrene];NSC166267;DTXSID20304552;JTVJHJFIEIFWQH-UHFFFAOYSA-N;9-dodecyl-tetradecahydro-phenanthrene;9-Dodecyltetradecahydrophenanthrene #;NSC-166267

Chemical Property of Phenanthrene, 9-dodecyltetradecahydro-

Chemical Property:

• Vapor Pressure: 6.09E-08mmHg at 25°C
• Refractive Index: 1.5220 (estimate)
• Boiling Point: 452.3°Cat760mmHg
• Flash Point: 214.4°C
• PSA: 0.00000
• Density: 0.873g/cm³
• LogP: 8.93010
• XLogP3: 12.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 11
• Exact Mass: 360.375601531
• Heavy Atom Count: 26
• Complexity: 359

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCC1CC2CCCCC2C3C1CCCC3

Technology Process of Phenanthrene, 9-dodecyltetradecahydro-

There total 5 articles about Phenanthrene, 9-dodecyltetradecahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-Docecyl-phenanthren (3788-61-2) → 9-Dodecyltetradecahydrophenanthrene (55334-01-5)

Guidance literature:

With nickel kieselguhr; at 100 - 230 ℃; under 51485.6 - 117681 Torr; Hydrogenation;

DOI:10.1021/ja01182a029

Reference yield:

lauric acid (143-07-7) → 9-Dodecyltetradecahydrophenanthrene (55334-01-5)

Guidance literature:

Multi-step reaction with 4 steps

1: phosphoric acid; NH₃ / 290 - 300 °C

2: diethyl ether; benzene / anschliessend Behandeln mit Eis und Schwefelsaeure

3: hydrazine hydrate; sodium methylate; ethanol / 200 °C

4: nickel kieselguhr / 100 - 230 °C / 51485.6 - 117681 Torr / Hydrogenation

With diethyl ether; ethanol; phosphoric acid; nickel kieselguhr; ammonia; sodium methylate; hydrazine hydrate; benzene;

DOI:10.1021/ja01182a029

Reference yield:

1-[9]phenanthryl-dodecan-1-one (412025-93-5) → 9-Dodecyltetradecahydrophenanthrene (55334-01-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate; sodium methylate; ethanol / 200 °C

2: nickel kieselguhr / 100 - 230 °C / 51485.6 - 117681 Torr / Hydrogenation

With ethanol; nickel kieselguhr; sodium methylate; hydrazine hydrate;

DOI:10.1021/ja01182a029

upstream raw materials:

9-Docecyl-phenanthren

lauric acid

1-[9]phenanthryl-dodecan-1-one

undecyl cyanide