2,4-DICHLOROBENZENE DIAZONIUM

Base Information

• Chemical Name: 2,4-DICHLOROBENZENE DIAZONIUM
• CAS No.: 27165-13-5
• Molecular Formula: C6H3 Cl2 N2
• Molecular Weight: 174.009
• Hs Code.: 2927000090
• Mol file: 27165-13-5.mol

Synonyms:2,4-Dichlorobenzenediazonium

Chemical Property of 2,4-DICHLOROBENZENE DIAZONIUM

Chemical Property:

• Vapor Pressure: 0.0971mmHg at 25°C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 28.15000
• Density: g/cm³
• LogP: 3.47798

Purity/Quality:

98.5% ^*data from raw suppliers

2,4-DICHLOROBENZENE DIAZONIUM 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-DICHLOROBENZENE DIAZONIUM

There total 5 articles about 2,4-DICHLOROBENZENE DIAZONIUM which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + acetic acid (64-19-7,77671-22-8) + 2,4-Dinitroanilin (97-02-9) → 2,4-Dichloro-benzenediazonium (27165-13-5) + 1-chloro-2,4-dinitro-benzene (97-00-7)

Guidance literature:

at 80 ℃; Geschwindigkeit der Reaktion;

Reference yield:

2,4-Dichloroaniline (554-00-7,51908-09-9) → 2,4-Dichloro-benzenediazonium (27165-13-5)

Guidance literature:

With sodium nitrite; In hydrogenchloride; water; at 5 ℃;

DOI:10.1016/S0045-6535(98)00582-7

Reference yield:

anti-2,4-Dichlorophenylazo methyl ether (73396-56-2) → 2,4-Dichloro-benzenediazonium (27165-13-5)

Guidance literature:

With sodium perchlorate; In methanol; at 30 ℃; Rate constant; var. subst. acetic acids and its salts as reagents;

upstream raw materials:

anti-2,4-Dichlorophenylazo methyl ether

2,4-Dichloroaniline

ethanol

chlorine

Downstream raw materials:

3-(2,4-dichloro-phenyl)-1-isopropyl-pyrrole-2,5-dione

2-(2,4-dichlorophenylsulfanyl)acetic acid

pentane-2,3,4-trione-3-(2,4-dichloro-phenylhydrazone)

(2,4-dichloro-phenylhydrazono)-malonyl chloride

Refernces

• 1、 Broxton, Trevor J.,Stray, Andrew C.. "Reactions of Aryldiazonium Salts and Alkyl Arylazo Ethers. VIII General Acid Catalysis of the Ionization of Alkyl (E)-Arylazo Ethers in Alcoholic Solvents". . p. 961 - 972. Retrieved 2007/10/02.