5,6-Dihydro-4,4,6-trimethyl-2-vinyl-4H-1,3-oxazine

Base Information

• Chemical Name: 5,6-Dihydro-4,4,6-trimethyl-2-vinyl-4H-1,3-oxazine
• CAS No.: 23878-88-8
• Molecular Formula: C9H15 N O
• Molecular Weight: 153.224
• Hs Code.: 2934999090
• European Community (EC) Number: 245-925-2
• NSC Number: 243028
• DSSTox Substance ID: DTXSID201218020
• Nikkaji Number: J242.695A
• Mol file: 23878-88-8.mol

Synonyms:23878-88-8;5,6-Dihydro-4,4,6-trimethyl-2-vinyl-4H-1,3-oxazine;2-ethenyl-4,4,6-trimethyl-5,6-dihydro-1,3-oxazine;5,6-DIHYDRO-4,4,6-TRIMETHYL-2-VINYL-1,3(4H)-OXAZINE;EINECS 245-925-2;2-Ethenyl-5,6-dihydro-4,4,6-trimethyl-4H-1,3-oxazine;4,4,6-trimethyl-2-vinyl-5,6-dihydro-4h-1,3-oxazine;NSC243028;SCHEMBL4572742;2-ethenyl-4,4,6-trimethyl-5,6-dihydro-4H-1,3-oxazine;DTXSID201218020;STL372877;AKOS006228278;NSC 243028;NSC-243028;FT-0619823;2-Vinyl-4,4,6-trimethyl-5,6-dihydro-1,3-[4H]oxazine;5,6-DIHYDRO-4,4,6-TRIMETHYL-2-VINYL-1,3-OXAZINE

Chemical Property of 5,6-Dihydro-4,4,6-trimethyl-2-vinyl-4H-1,3-oxazine

Chemical Property:

• Vapor Pressure: 3.04mmHg at 25°C
• Boiling Point: 160.9°Cat760mmHg
• Flash Point: 46°C
• PSA: 21.59000
• Density: 0.94g/cm³
• LogP: 1.59390
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 153.115364102
• Heavy Atom Count: 11
• Complexity: 194

Purity/Quality:

99% ^*data from raw suppliers

5,6-DIHYDRO-4,4,6-TRIMETHYL-2-VINYL-1,3-OXAZINE Aldrich ^*data from reagent suppliers

Safty Information:

• Statements: R36/38:Irritating to eyes and skin.
• Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S36:Wear suitable prot

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CC(N=C(O1)C=C)(C)C

Technology Process of 5,6-Dihydro-4,4,6-trimethyl-2-vinyl-4H-1,3-oxazine

There total 3 articles about 5,6-Dihydro-4,4,6-trimethyl-2-vinyl-4H-1,3-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-2,4-pentanediol (107-41-5) + acrylonitrile (107-13-1,25014-41-9) → 4,4,6-trimethyl-2-vinyl-5,6-dihydro-4H-[1,3]oxazine (23878-88-8)

Guidance literature:

With sulfuric acid;

DOI:10.1021/jo01087a613

Reference yield:

2-methyl-2,4-pentanediol (107-41-5) + sulfuric acid (7664-93-9) + acrylonitrile (107-13-1,25014-41-9) → 4,4,6-trimethyl-2-vinyl-5,6-dihydro-4H-[1,3]oxazine (23878-88-8)

Guidance literature:

DOI:10.1021/jo01087a613

Reference yield:

→ 4,4,6-trimethyl-2-vinyl-5,6-dihydro-4H-[1,3]oxazine (23878-88-8)

Guidance literature:

2-Methyl-2,4-pentandiol, Acrylnitril, H2SO4;

DOI:10.1021/jo00941a008

upstream raw materials:

2-methyl-2,4-pentanediol

acrylonitrile

sulfuric acid

Downstream raw materials:

4-Hydroxy-2-benzyl-4-phenyl-butanal

2-[2-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-ethyl]-cyclopentanone

2-[2-(1,4-dioxa-spiro[4.4]non-6-yl)-ethyl]-4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazine

2-(3,4-Dimethyl-cyclohex-3-enyl)-4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazine