Technology Process of 4-Azidoaniline
There total 17 articles about 4-Azidoaniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-bromo-aniline;
With
copper(l) iodide; sodium L-ascorbate; N,N`-dimethylethylenediamine;
In
ethanol; water;
for 0.166667h;
Inert atmosphere;
With
sodium azide;
In
ethanol; water;
for 3h;
Inert atmosphere;
Reflux;
DOI:10.1002/adsc.201200856
- Guidance literature:
-
With
copper(l) iodide; sodium azide; N,N,N,N,-tetramethylethylenediamine; sodium hydroxide; ascorbic acid;
In
ethanol; water;
at 20 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1016/j.tet.2010.01.028
- Guidance literature:
-
With
sodium azide; copper diacetate;
In
methanol;
at 55 ℃;
for 24h;
DOI:10.1055/s-0029-1218683
