Technology Process of Beryllium dimethanide
There total 13 articles about Beryllium dimethanide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
diethyl ether;
byproducts: LiCl; all manipulation under N2O/He or Ar; 2 equiv MeLi soln. added dropwise to prepurified BeCl2 suspn. over 2 h with vigorous stirring; LiCl filtered, filtrate evapd. in vac., solid dried in vac. overnight, purifd. by sublimation;
- Guidance literature:
-
With
beryllium;
at 130 ℃;
im Rohr;
- Guidance literature:
-
In
gaseous matrix;
codeposition of laser-ablated Be and ethane;
DOI:10.1021/ja9804870