Technology Process of 1-(2-Aminophenyl)-2-(2-bromophenyl)ethanone
There total 3 articles about 1-(2-Aminophenyl)-2-(2-bromophenyl)ethanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid;
at 20 ℃;
for 0.166667h;
DOI:10.1021/ol051291p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 86 percent / cesium carbonate; Xantphos / palladium(II) acetate / toluene; H2O / 48 h / 120 °C
2: 95 percent / sulfuric acid / 0.17 h / 20 °C
With
sulfuric acid; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
palladium diacetate;
In
water; toluene;
DOI:10.1016/j.tet.2006.11.003
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 96 percent / pyridine / CH2Cl2 / 20 °C
2: 86 percent / cesium carbonate; Xantphos / palladium(II) acetate / toluene; H2O / 48 h / 120 °C
3: 95 percent / sulfuric acid / 0.17 h / 20 °C
With
pyridine; sulfuric acid; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
palladium diacetate;
In
dichloromethane; water; toluene;
DOI:10.1016/j.tet.2006.11.003