S-(4-chlorobenzyl) methylcarbamothioate

Base Information

• Chemical Name: S-(4-chlorobenzyl) methylcarbamothioate
• CAS No.: 92988-97-1
• Molecular Formula: C9H10 Cl N O S
• Molecular Weight: 215.6998
• Mol file: 92988-97-1.mol

Synonyms:Carbamic acid, methylthio-, S-p-chlorobenzyl ester (7CI); NSC 35978

Chemical Property of S-(4-chlorobenzyl) methylcarbamothioate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.264g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of S-(4-chlorobenzyl) methylcarbamothioate

There total 2 articles about S-(4-chlorobenzyl) methylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.3%

N-Methyl-O-phenylcarbamat (1943-79-9) + (4-chlorophenyl)methanethiol (6258-66-8) → S-(4-chlorobenzyl)methylthiocarbamate (92988-97-1)

Guidance literature:

With tributylphosphine; potassium carbonate; In acetonitrile; at 20 ℃; for 4h;

DOI:10.1055/s-2006-950353

Reference yield:

→ S-(4-chlorobenzyl)methylthiocarbamate (92988-97-1)

Guidance literature:

Aus dem Saeurechlorid und Amin;

Reference yield: 98.7%

S-(4-chlorobenzyl)methylthiocarbamate (92988-97-1) → 4-chlorobenzylsulfonyl chloride (6966-45-6)

Guidance literature:

With hydrogenchloride; N-chloro-succinimide; In acetonitrile; at 10 ℃;

DOI:10.1055/s-2006-950353

upstream raw materials:

N-Methyl-O-phenylcarbamat

(4-chlorophenyl)methanethiol

Downstream raw materials:

4-chlorobenzylsulfonyl chloride

Refernces