Heptadecylamine

Base Information

• Chemical Name: Heptadecylamine
• CAS No.: 4200-95-7
• Molecular Formula: C17H37N
• Molecular Weight: 255.487
• Hs Code.: 2921199090
• European Community (EC) Number: 224-103-7
• NSC Number: 91524
• UNII: 4YG9UE6EH0
• DSSTox Substance ID: DTXSID1063350
• Nikkaji Number: J106.588B
• Wikidata: Q27260667
• Mol file: 4200-95-7.mol

Synonyms:1-Aminoheptadecane;Heptadecylamine;4200-95-7;1-Heptadecanamine;heptadecan-1-amine;Margarylamine;n-Heptadecylamine;UNII-4YG9UE6EH0;4YG9UE6EH0;EINECS 224-103-7;NSC 91524;NSC-91524;9-octylnonylamine;NSC91524;SCHEMBL37327;DTXSID1063350;C17H37N;MFCD00053647;AKOS015894493;A0764;FT-0607344;T70904;A825715;Q27260667

Chemical Property of Heptadecylamine

Chemical Property:

• Vapor Pressure: 0.000118mmHg at 25°C
• Melting Point: 46 °C
• Refractive Index: 1.451
• Boiling Point: 335.7 °C at 760 mmHg
• PKA: 10.67±0.10(Predicted)
• Flash Point: 146.2 °C
• PSA: 26.02000
• Density: 0.816 g/cm³
• LogP: 6.51680
• Solubility.: soluble in Methanol
• XLogP3: 8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 15
• Exact Mass: 255.292600184
• Heavy Atom Count: 18
• Complexity: 134

Purity/Quality:

98% ^*data from raw suppliers

1-Aminoheptadecane ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Nitrogen Compounds -> Amines, Aliphatic
• Canonical SMILES: CCCCCCCCCCCCCCCCCN

Technology Process of Heptadecylamine

There total 15 articles about Heptadecylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

heptadecanenitrile (5399-02-0) → 1-heptadecanamine (4200-95-7)

Guidance literature:

With ammonia; hydrogen; In water; isopropyl alcohol; at 80 ℃; for 24h; under 15001.5 Torr; Autoclave;

DOI:10.1002/chem.202001866

Reference yield: 75.0%

bis(1-nitrosoheptadecane) → 1-heptadecanamine (4200-95-7)

Guidance literature:

With hydrogen; platinum(IV) oxide;

DOI:10.1039/c39950002385

Reference yield:

eicosan-3-one oxime (116557-12-1) + sulfuric acid (7664-93-9) + acetic acid (64-19-7,77671-22-8) → 1-heptadecanamine (4200-95-7) + stearic acid (57-11-4)

Guidance literature:

higher-melting form; und Verseifen mit alkoh.KOH;

upstream raw materials:

heptadecyl isocyanate

heptadecyl-carbamic acid methyl ester

dichloromethane

stearic acid

Downstream raw materials:

N-heptadecyl-2,4,6-trinitroaniline

C₃₄H₅₇N₃O₄S

Refernces

• 1、 Booth,Norrish. "". . p. 188,193,194,196. Retrieved 1952.
• 2、 Formenti, Dario,Mocci, Rita,Atia, Hanan,Dastgir, Sarim,Anwar, Muhammad,Bachmann, Stephan,Scalone, Michelangelo,Junge, Kathrin,Beller, Matthias. "A State-of-the-Art Heterogeneous Catalyst for Efficient and General Nitrile Hydrogenation". supporting information. p. 15589 - 15595. Retrieved 2020/10/02.
• 3、 Girard, Pierre,Guillot, Nadine,Motherwell, William B.,Hay-Motherwell, Robyn S.,Potier, Pierre. "The reaction of thionitrites with Barton esters: A convenient free radical chain reaction for decarboxylative nitrosation". . p. 3573 - 3584. Retrieved 2007/10/03.