9,10-Dihydro-9,10,10-triphenyl-9-anthrol

Base Information

• Chemical Name: 9,10-Dihydro-9,10,10-triphenyl-9-anthrol
• CAS No.: 6636-11-9
• Molecular Formula: C32H24 O
• Molecular Weight: 424.542
• Hs Code.: 2906299090
• Mol file: 6636-11-9.mol

Synonyms:9-Anthrol,9,10-dihydro-9,10,10-triphenyl- (6CI,8CI); NSC 16441

Chemical Property of 9,10-Dihydro-9,10,10-triphenyl-9-anthrol

Chemical Property:

• Vapor Pressure: 3.89E-13mmHg at 25°C
• Boiling Point: 554.6°Cat760mmHg
• Flash Point: 228.5°C
• PSA: 20.23000
• Density: 1.204g/cm³
• LogP: 6.66690

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9,10-Dihydro-9,10,10-triphenyl-9-anthrol

There total 10 articles about 9,10-Dihydro-9,10,10-triphenyl-9-anthrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

bromobenzene (108-86-1,52753-63-6) + 10,10-Diphenyl-10H-anthracen-9-one (3216-03-3) → 9,10,10-Triphenyl-9,10-dihydro-[9]anthrol (6636-11-9)

Guidance literature:

bromobenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 3h; Inert atmosphere;

10,10-Diphenyl-10H-anthracen-9-one; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

9,9,10-Triphenyl-10-hydroperoxy-9,10-dihydroanthracen (6549-72-0) → 9,10,10-Triphenyl-9,10-dihydro-[9]anthrol (6636-11-9)

Guidance literature:

With hydrogen; platinum(IV) oxide; In methanol;

Reference yield:

9.9.10-Triphenyl-8a.9-dihydro-anthracen (6549-73-1) → 9,10,10-Triphenyl-9,10-dihydro-[9]anthrol (6636-11-9)

Guidance literature:

Multi-step reaction with 2 steps

1: O₂ / benzene

2: H₂ / PtO₂ / methanol

With hydrogen; oxygen; platinum(IV) oxide; In methanol; benzene;

upstream raw materials:

diethyl ether

10,10-Diphenyl-10H-anthracen-9-one

9,9,10-Triphenyl-10-hydroperoxy-9,10-dihydroanthracen

9.9.10-Triphenyl-8a.9-dihydro-anthracen

Downstream raw materials:

9,9,10-triphenyl-9,10-dihydro-anthracene

9-chloro-9,10,10-triphenyl-9,10-dihydro-anthracene

Refernces