Technology Process of Tetradecanedioic acid, monoethyl ester
There total 1 articles about Tetradecanedioic acid, monoethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid;
In
cyclohexane; water;
for 24h;
DOI:10.1021/la204412t
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 89 percent / BH3, Me2S / tetrahydrofuran
2: 88 percent / KOH / methanol; H2O
3: 79 percent / PPh3 / tetrahydrofuran
4: 70 percent / (COCl)2, DMSO, Et3N
5: 71 percent / toluene / Ambient temperature
6: 57 percent / xylene / 24 h / Heating
7: 2.) toluene, -10 deg C
8: LiAlH4
9: Jones reagent
10: 50 °C
With
potassium hydroxide; lithium aluminium tetrahydride; jones reagent; oxalyl dichloride; dimethylsulfide; borane; dimethyl sulfoxide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; water; toluene; xylene;
DOI:10.1039/c39910001438
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 89 percent / BH3, Me2S / tetrahydrofuran
2: 88 percent / KOH / methanol; H2O
3: 79 percent / PPh3 / tetrahydrofuran
4: 70 percent / (COCl)2, DMSO, Et3N
5: 71 percent / toluene / Ambient temperature
6: 57 percent / xylene / 24 h / Heating
7: 2.) toluene, -10 deg C
With
potassium hydroxide; oxalyl dichloride; dimethylsulfide; borane; dimethyl sulfoxide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; water; toluene; xylene;
DOI:10.1039/c39910001438
