Technology Process of 1,3,5-Trifluoro-2,4-diiodo-6-nitrobenzene
There total 1 articles about 1,3,5-Trifluoro-2,4-diiodo-6-nitrobenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuric acid; periodic acid; potassium iodide;
at 0 - 50 ℃;
for 4h;
DOI:10.1021/jo061624b
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
for 1h;
under 3000.24 Torr;
DOI:10.1021/jo061624b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / hydrogen / palladium on carbon / methanol / 1 h / 3000.24 Torr
2: 650 mg / trifluoroacetic acid; sodium nitrite / H2O / 0.5 h / -5 °C
3: Photolysis
With
hydrogen; trifluoroacetic acid; sodium nitrite;
palladium on activated charcoal;
In
methanol; water;
DOI:10.1021/jo061624b